Technology Process of C22H25F3O4
There total 3 articles about C22H25F3O4 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
sodium hydrogencarbonate; Dess-Martin periodane;
In
dichloromethane;
at 20 ℃;
DOI:10.1246/cl.131099
- Guidance literature:
-
Multi-step reaction with 4 steps
1: scandium tris(trifluoromethanesulfonate) / toluene / 20 °C
2: diisobutylaluminium hydride / dichloromethane / -78 °C
3: tetrabutyl ammonium fluoride / tetrahydrofuran / 20 °C
4: Dess-Martin periodane; sodium hydrogencarbonate / dichloromethane / 20 °C
With
tetrabutyl ammonium fluoride; diisobutylaluminium hydride; sodium hydrogencarbonate; Dess-Martin periodane; scandium tris(trifluoromethanesulfonate);
In
tetrahydrofuran; dichloromethane; toluene;
4: |Dess-Martin Oxidation;
DOI:10.1246/cl.131099
- Guidance literature:
-
Multi-step reaction with 4 steps
1: scandium tris(trifluoromethanesulfonate) / toluene / 20 °C
2: diisobutylaluminium hydride / dichloromethane / -78 °C
3: tetrabutyl ammonium fluoride / tetrahydrofuran / 20 °C
4: Dess-Martin periodane; sodium hydrogencarbonate / dichloromethane / 20 °C
With
tetrabutyl ammonium fluoride; diisobutylaluminium hydride; sodium hydrogencarbonate; Dess-Martin periodane; scandium tris(trifluoromethanesulfonate);
In
tetrahydrofuran; dichloromethane; toluene;
4: |Dess-Martin Oxidation;
DOI:10.1246/cl.131099