(S)-3,4-Bis-benzyloxy-5-((R)-2,2-dimethyl-[1,3]dioxolan-4-yl)-5H-furan-2-one

Base Information

Chemical Name:(S)-3,4-Bis-benzyloxy-5-((R)-2,2-dimethyl-[1,3]dioxolan-4-yl)-5H-furan-2-one
CAS No.:185683-67-4
Molecular Formula:C₂₃H₂₄O₆
Molecular Weight:396.44
Hs Code.:

Synonyms:(S)-3,4-Bis-benzyloxy-5-((R)-2,2-dimethyl-[1,3]dioxolan-4-yl)-5H-furan-2-one

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Chemical Property of (S)-3,4-Bis-benzyloxy-5-((R)-2,2-dimethyl-[1,3]dioxolan-4-yl)-5H-furan-2-one

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Technology Process of (S)-3,4-Bis-benzyloxy-5-((R)-2,2-dimethyl-[1,3]dioxolan-4-yl)-5H-furan-2-one

There total 1 articles about (S)-3,4-Bis-benzyloxy-5-((R)-2,2-dimethyl-[1,3]dioxolan-4-yl)-5H-furan-2-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 122046-90-6
O²,O³-dibenzyl-O⁵,O⁶-isopropyliden-L-ascorbic acid

: 136767-82-3
3,4-dibenzyloxy-5-(2-hydroxyethylidene)-2(5H)-furanone

: 185683-67-4
(S)-3,4-Bis-benzyloxy-5-((R)-2,2-dimethyl-[1,3]dioxolan-4-yl)-5H-furan-2-one

Guidance literature:: With triisobutylaluminum; In toluene; at 100 ℃; for 72h; Mechanism; other ascorbic and isoascorbic acid derivatives;
DOI:10.1016/0957-4166(96)00427-2

Reference yield: 84.0%

: 185683-67-4
(S)-3,4-Bis-benzyloxy-5-((R)-2,2-dimethyl-[1,3]dioxolan-4-yl)-5H-furan-2-one

: 185675-44-9
Oxalic acid benzyl ester (S)-benzyloxycarbonyl-((R)-2,2-dimethyl-[1,3]dioxolan-4-yl)-methyl ester

Guidance literature:: With ozone; In dichloromethane;
DOI:10.1016/0957-4166(96)00427-2

Reference yield:

: 185683-67-4
(S)-3,4-Bis-benzyloxy-5-((R)-2,2-dimethyl-[1,3]dioxolan-4-yl)-5H-furan-2-one

: (S)-((R)-2,2-Dimethyl-[1,3]dioxolan-4-yl)-hydroxy-acetic acid benzyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 84 percent / O₃ / CH₂Cl₂

2: 66 percent / methanol / 4 h / Heating

With ozone; In methanol; dichloromethane;
DOI:10.1016/0957-4166(96)00427-2