tert-butyl 2-{1-[chloro(p-tolylsulfinyl)methyl]cyclopentadecyl}butanoate

Base Information

Chemical Name:tert-butyl 2-{1-[chloro(p-tolylsulfinyl)methyl]cyclopentadecyl}butanoate
CAS No.:867150-94-5
Molecular Formula:C₃₁H₅₁ClO₃S
Molecular Weight:539.263
Hs Code.:

Synonyms:tert-butyl 2-{1-[chloro(p-tolylsulfinyl)methyl]cyclopentadecyl}butanoate

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Chemical Property of tert-butyl 2-{1-[chloro(p-tolylsulfinyl)methyl]cyclopentadecyl}butanoate

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Technology Process of tert-butyl 2-{1-[chloro(p-tolylsulfinyl)methyl]cyclopentadecyl}butanoate

There total 2 articles about tert-butyl 2-{1-[chloro(p-tolylsulfinyl)methyl]cyclopentadecyl}butanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: [Chloro-((R)-toluene-4-sulfinyl)-methylene]-cyclopentadecane

: 2308-38-5
tert-butyl butyrate

: 867150-94-5
tert-butyl 2-{1-[chloro(p-tolylsulfinyl)methyl]cyclopentadecyl}butanoate

Guidance literature:: tert-butyl butyrate; With lithium diisopropyl amide; In tetrahydrofuran; at -75 ℃;

[Chloro-((R)-toluene-4-sulfinyl)-methylene]-cyclopentadecane; In tetrahydrofuran;
DOI:10.1016/j.tetlet.2005.06.172

Reference yield:

: [Chloro-((R)-toluene-4-sulfinyl)-methylene]-cyclopentadecane

: 2308-38-5
tert-butyl butyrate

: 867150-94-5
tert-butyl 2-{1-[chloro(p-tolylsulfinyl)methyl]cyclopentadecyl}butanoate

: tert-butyl 2-{1-[chloro(p-tolylsulfinyl)methyl]cyclopentadecyl}butanoate

Guidance literature:: tert-butyl butyrate; With N,N,N,N,N,N-hexamethylphosphoric triamide; lithium diisopropyl amide; In tetrahydrofuran; at -75 ℃;

[Chloro-((R)-toluene-4-sulfinyl)-methylene]-cyclopentadecane; In tetrahydrofuran; at -75 - -50 ℃; Further stages. Title compound not separated from byproducts.;
DOI:10.1016/j.tetasy.2007.07.033