1,4-dimethyl-7-tert-butyl-8-hydroxy-10-(3',5'-di-tert-butyl-4'-hydroxyphenyl)-5,10-dihydrobenzophthalazine trifluoroacetate

Base Information

Chemical Name:1,4-dimethyl-7-tert-butyl-8-hydroxy-10-(3',5'-di-tert-butyl-4'-hydroxyphenyl)-5,10-dihydrobenzophthalazine trifluoroacetate
CAS No.:111534-91-9
Molecular Formula:C₂HF₃O₂*C₃₂H₄₂N₂O₂
Molecular Weight:600.722
Hs Code.:

1,4-dimethyl-7-tert-butyl-8-hydroxy-10-(3',5'-di-tert-butyl-4'-hydroxyphenyl)-5,10-dihydrobenzo<g>phthalazine trifluoroacetate

Synonyms:1,4-dimethyl-7-tert-butyl-8-hydroxy-10-(3',5'-di-tert-butyl-4'-hydroxyphenyl)-5,10-dihydrobenzophthalazine trifluoroacetate

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Chemical Property of 1,4-dimethyl-7-tert-butyl-8-hydroxy-10-(3',5'-di-tert-butyl-4'-hydroxyphenyl)-5,10-dihydrobenzophthalazine trifluoroacetate

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Technology Process of 1,4-dimethyl-7-tert-butyl-8-hydroxy-10-(3',5'-di-tert-butyl-4'-hydroxyphenyl)-5,10-dihydrobenzophthalazine trifluoroacetate

There total 3 articles about 1,4-dimethyl-7-tert-butyl-8-hydroxy-10-(3',5'-di-tert-butyl-4'-hydroxyphenyl)-5,10-dihydrobenzophthalazine trifluoroacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 111512-68-6
3,5-di-tert-butyl-4-oxo-3',6'-dimethyl-7'-(3'',5''-di-tert-butyl-4''-hydroxyphenyl)spiro<2,5-cyclohexadiene-1,1'-cyclopentapyridazine>

: 76-05-1
trifluoroacetic acid

: 111534-91-9
1,4-dimethyl-7-tert-butyl-8-hydroxy-10-(3',5'-di-tert-butyl-4'-hydroxyphenyl)-5,10-dihydrobenzophthalazine trifluoroacetate

Guidance literature:: for 12h; Ambient temperature;

Reference yield:

: 111534-90-8
3,4-Di(3,5-di-tert-butyl-5-hydroxybenzylidene)hexane-2,5-dione

: 111534-91-9
1,4-dimethyl-7-tert-butyl-8-hydroxy-10-(3',5'-di-tert-butyl-4'-hydroxyphenyl)-5,10-dihydrobenzophthalazine trifluoroacetate

Guidance literature:: Multi-step reaction with 2 steps

1: 99 percent / hydrazine hydrate / ethanol / 0.5 h / 80 °C

2: 78 percent / 12 h / Ambient temperature

With hydrazine hydrate; In ethanol;

Reference yield:

: 111512-69-7
2,3-Diacetyl-4-(3,5-di-tert-butyl-4-hydroxyphenyl)spiro<4,5>deca-1,6,9-trien-8-one

: 111534-91-9
1,4-dimethyl-7-tert-butyl-8-hydroxy-10-(3',5'-di-tert-butyl-4'-hydroxyphenyl)-5,10-dihydrobenzophthalazine trifluoroacetate

Guidance literature:: Multi-step reaction with 2 steps

1: 0.03 g / hydrazine hydrate / ethanol / 30 h / 60 °C

2: 78 percent / 12 h / Ambient temperature

With hydrazine hydrate; In ethanol;