[perchlorato-bis[benzimidazole-2-N-(4-methoxyphenyl)carbothioamidato]copper(III)] hydroperchlorate

Base Information

Chemical Name:[perchlorato-bis[benzimidazole-2-N-(4-methoxyphenyl)carbothioamidato]copper(III)] hydroperchlorate
CAS No.:860774-59-0
Molecular Formula:C₃₀H₂₄ClCuN₆O₆S₂*ClHO₄
Molecular Weight:828.147
Hs Code.:

Synonyms:[perchlorato-bis[benzimidazole-2-N-(4-methoxyphenyl)carbothioamidato]copper(III)] hydroperchlorate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of [perchlorato-bis[benzimidazole-2-N-(4-methoxyphenyl)carbothioamidato]copper(III)] hydroperchlorate

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Technology Process of [perchlorato-bis[benzimidazole-2-N-(4-methoxyphenyl)carbothioamidato]copper(III)] hydroperchlorate

There total 1 articles about [perchlorato-bis[benzimidazole-2-N-(4-methoxyphenyl)carbothioamidato]copper(III)] hydroperchlorate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 7601-90-3
perchloric acid

: cooper(II) monochloroacetate dihydrate

: 157116-96-6
benzimidazole-2-N-(4-methoxyphenyl)carbothioamide

: 860774-59-0
[perchlorato-bis[benzimidazole-2-N-(4-methoxyphenyl)carbothioamidato]copper(III)] hydroperchlorate

Guidance literature:: With air; HOAc; Ac₂O; In methanol; ethanol; byproducts: H2O; hot soln. of benzimidazole-2-N-(4-methoxyphenyl)carbothioamide(HL) in anhyd. EtOH mixed with soln. of Cu(ClCH2COO)2*2H2O in anhyd. MeOH; to suspn. of CuL2 added HClO4, HOAc, Ac2O; mixt. became hot and ppt. dissolved;ratio HL:Cu:HClO4=2:1:16; soln. cooled to room temp. and crystals slow pptd.; crystals filtered off, washed several times with ethanol and dried in air; elem. anal.;
DOI:10.1007/s11173-005-0042-1