2,5-bis[(3,5-bis{[4-(tert-butyl)benzyl]oxy}benzyl)oxy]-1,4-diiodobenzene

Base Information

Chemical Name:2,5-bis[(3,5-bis{[4-(tert-butyl)benzyl]oxy}benzyl)oxy]-1,4-diiodobenzene
CAS No.:929803-61-2
Molecular Formula:C₆₄H₇₂I₂O₆
Molecular Weight:1191.08
Hs Code.:

Synonyms:2,5-bis[(3,5-bis{[4-(tert-butyl)benzyl]oxy}benzyl)oxy]-1,4-diiodobenzene

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Chemical Property of 2,5-bis[(3,5-bis{[4-(tert-butyl)benzyl]oxy}benzyl)oxy]-1,4-diiodobenzene

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Technology Process of 2,5-bis[(3,5-bis{[4-(tert-butyl)benzyl]oxy}benzyl)oxy]-1,4-diiodobenzene

There total 8 articles about 2,5-bis[(3,5-bis{[4-(tert-butyl)benzyl]oxy}benzyl)oxy]-1,4-diiodobenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 13064-64-7
2,5-diiodo-1,4-hydroquinone

: 339531-03-2
5-(bromomethyl)-1,3-bis{[4-(tert-butyl)benzyl]oxy}benzene

: 929803-61-2
2,5-bis[(3,5-bis{[4-(tert-butyl)benzyl]oxy}benzyl)oxy]-1,4-diiodobenzene

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 50 ℃; for 4h;
DOI:10.1021/ol062793l

Reference yield:

: 916226-09-0
2,5-bis(methoxymethoxy)-1,4-diiodobenzene

: 929803-61-2
2,5-bis[(3,5-bis{[4-(tert-butyl)benzyl]oxy}benzyl)oxy]-1,4-diiodobenzene

Guidance literature:: Multi-step reaction with 2 steps

1: 95 percent / aq. HCl; methanol / 4 h / Heating

2: 84 percent / potassium carbonate / dimethylformamide / 4 h / 50 °C

With hydrogenchloride; methanol; potassium carbonate; In N,N-dimethyl-formamide;
DOI:10.1021/ol062793l

Reference yield:

: 2150-44-9
1-carbomethoxy-3,5-dihydroxybenzene

: 929803-61-2
2,5-bis[(3,5-bis{[4-(tert-butyl)benzyl]oxy}benzyl)oxy]-1,4-diiodobenzene

Guidance literature:: Multi-step reaction with 4 steps

1: 89 percent / potassium carbonate; 18-crown-6 / acetone / 48 h / Heating

2: 90 percent / LiAlH₄ / tetrahydrofuran / 4 h / 20 °C

3: 95 percent / carbon tetrabromide; triphenylphosphine / tetrahydrofuran / 4 h / 20 °C

4: 84 percent / potassium carbonate / dimethylformamide / 4 h / 50 °C

With lithium aluminium tetrahydride; 18-crown-6 ether; carbon tetrabromide; potassium carbonate; triphenylphosphine; In tetrahydrofuran; N,N-dimethyl-formamide; acetone;
DOI:10.1021/ol062793l