Technology Process of C24H20F6N2O3
There total 9 articles about C24H20F6N2O3 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
3,5-Bis-(trifluoromethyl)aniline;
With
n-butyllithium;
In
tetrahydrofuran;
at -78 - 20 ℃;
C17H19NO4;
In
tetrahydrofuran;
at 75 ℃;
for 2h;
- Guidance literature:
-
Multi-step reaction with 8 steps
1.1: 0.75 h / 130 °C
2.1: acetyl chloride / 1 h / 64 °C
3.1: lithium hexamethyldisilazane / tetrahydrofuran / 0.17 h / -50 °C
3.2: 1 h / -50 - 20 °C
4.1: sodium hydride / tetrahydrofuran; mineral oil / 18 h / 0 - 20 °C
5.1: lithium hexamethyldisilazane / tetrahydrofuran / 1 h / -78 °C
6.1: sodium tetrahydroborate / tetrahydrofuran / 1 h / 0 - 20 °C
7.1: Burgess Reagent / tetrahydrofuran / 2 h / 75 °C
8.1: n-butyllithium / tetrahydrofuran / -78 - 20 °C
8.2: 2 h / 75 °C
With
sodium tetrahydroborate; n-butyllithium; Burgess Reagent; sodium hydride; acetyl chloride; lithium hexamethyldisilazane;
In
tetrahydrofuran; mineral oil;
- Guidance literature:
-
Multi-step reaction with 8 steps
1.1: 0.75 h / 130 °C
2.1: acetyl chloride / 1 h / 64 °C
3.1: lithium hexamethyldisilazane / tetrahydrofuran / 0.17 h / -50 °C
3.2: 1 h / -50 - 20 °C
4.1: sodium hydride / tetrahydrofuran; mineral oil / 18 h / 0 - 20 °C
5.1: lithium hexamethyldisilazane / tetrahydrofuran / 1 h / -78 °C
6.1: sodium tetrahydroborate / tetrahydrofuran / 1 h / 0 - 20 °C
7.1: Burgess Reagent / tetrahydrofuran / 2 h / 75 °C
8.1: n-butyllithium / tetrahydrofuran / -78 - 20 °C
8.2: 2 h / 75 °C
With
sodium tetrahydroborate; n-butyllithium; Burgess Reagent; sodium hydride; acetyl chloride; lithium hexamethyldisilazane;
In
tetrahydrofuran; mineral oil;