[(R)-2-Benzyloxy-1-(2,3,5-trimethoxy-4-methyl-phenyl)-ethyl]-(2,2-diethoxy-ethyl)-amine

Base Information

Chemical Name:[(R)-2-Benzyloxy-1-(2,3,5-trimethoxy-4-methyl-phenyl)-ethyl]-(2,2-diethoxy-ethyl)-amine
CAS No.:271578-84-8
Molecular Formula:C₂₅H₃₇NO₆
Molecular Weight:447.572
Hs Code.:

Synonyms:[(R)-2-Benzyloxy-1-(2,3,5-trimethoxy-4-methyl-phenyl)-ethyl]-(2,2-diethoxy-ethyl)-amine

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Chemical Property of [(R)-2-Benzyloxy-1-(2,3,5-trimethoxy-4-methyl-phenyl)-ethyl]-(2,2-diethoxy-ethyl)-amine

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Technology Process of [(R)-2-Benzyloxy-1-(2,3,5-trimethoxy-4-methyl-phenyl)-ethyl]-(2,2-diethoxy-ethyl)-amine

There total 13 articles about [(R)-2-Benzyloxy-1-(2,3,5-trimethoxy-4-methyl-phenyl)-ethyl]-(2,2-diethoxy-ethyl)-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 271578-78-0
1,3,4-trimethoxy-2-methyl-5-vinylbenzene

: 271578-84-8
[(R)-2-Benzyloxy-1-(2,3,5-trimethoxy-4-methyl-phenyl)-ethyl]-(2,2-diethoxy-ethyl)-amine

Guidance literature:: Multi-step reaction with 5 steps

1: 5.2 g / NaH; n-Bu₄NI / tetrahydrofuran / 12 h / 20 °C

2: 7.37 g / H₂ / Pd/C / ethyl acetate / 5 h / 760.05 Torr

3: TFA / CH₂Cl₂ / 1 h / 20 °C

4: 5.0 g / K₂CO₃ / acetonitrile / 72 h / Heating

With hydrogen; tetra-(n-butyl)ammonium iodide; sodium hydride; potassium carbonate; trifluoroacetic acid; palladium on activated charcoal; In tetrahydrofuran; dichloromethane; ethyl acetate; acetonitrile;
DOI:10.1021/ol016844k

Reference yield:

: (R)-2-Azido-2-(2,3,5-trimethoxy-4-methyl-phenyl)-ethanol

: 271578-84-8
[(R)-2-Benzyloxy-1-(2,3,5-trimethoxy-4-methyl-phenyl)-ethyl]-(2,2-diethoxy-ethyl)-amine

Guidance literature:: Multi-step reaction with 4 steps

1: 5.2 g / NaH; n-Bu₄NI / tetrahydrofuran / 12 h / 20 °C

2: 7.37 g / H₂ / Pd/C / ethyl acetate / 5 h / 760.05 Torr

3: TFA / CH₂Cl₂ / 1 h / 20 °C

4: 5.0 g / K₂CO₃ / acetonitrile / 72 h / Heating

With hydrogen; tetra-(n-butyl)ammonium iodide; sodium hydride; potassium carbonate; trifluoroacetic acid; palladium on activated charcoal; In tetrahydrofuran; dichloromethane; ethyl acetate; acetonitrile;
DOI:10.1021/ol016844k

Reference yield:

: 1-((R)-1-Azido-2-benzyloxy-ethyl)-2,3,5-trimethoxy-4-methyl-benzene

: 271578-84-8
[(R)-2-Benzyloxy-1-(2,3,5-trimethoxy-4-methyl-phenyl)-ethyl]-(2,2-diethoxy-ethyl)-amine

Guidance literature:: Multi-step reaction with 3 steps

1: 7.37 g / H₂ / Pd/C / ethyl acetate / 5 h / 760.05 Torr

2: TFA / CH₂Cl₂ / 1 h / 20 °C

3: 5.0 g / K₂CO₃ / acetonitrile / 72 h / Heating

With hydrogen; potassium carbonate; trifluoroacetic acid; palladium on activated charcoal; In dichloromethane; ethyl acetate; acetonitrile;
DOI:10.1021/ol016844k