3-nitrophenyl N-bis(dimethylamino)methylene-N'-phenylcarbamimidothioate

Base Information

Chemical Name:3-nitrophenyl N-bis(dimethylamino)methylene-N'-phenylcarbamimidothioate
CAS No.:1564286-41-4
Molecular Formula:C₁₈H₂₁N₅O₂S
Molecular Weight:371.463
Hs Code.:

Synonyms:3-nitrophenyl N-bis(dimethylamino)methylene-N'-phenylcarbamimidothioate

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Chemical Property of 3-nitrophenyl N-bis(dimethylamino)methylene-N'-phenylcarbamimidothioate

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Technology Process of 3-nitrophenyl N-bis(dimethylamino)methylene-N'-phenylcarbamimidothioate

There total 3 articles about 3-nitrophenyl N-bis(dimethylamino)methylene-N'-phenylcarbamimidothioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 585-79-5
m-nitrobromobenzene

: 84764-54-5
C₁₂H₁₈N₄S

: 1564286-41-4
3-nitrophenyl N-bis(dimethylamino)methylene-N'-phenylcarbamimidothioate

Guidance literature:: With copper(l) iodide; 1,10-Phenanthroline; potassium carbonate; In N,N-dimethyl-formamide; at 110 ℃; for 10h; Inert atmosphere;
DOI:10.1016/j.tetlet.2014.01.006

Reference yield:

: 80-70-6
N,N,N',N'-tetramethylguanidine

: 1564286-41-4
3-nitrophenyl N-bis(dimethylamino)methylene-N'-phenylcarbamimidothioate

Guidance literature:: Multi-step reaction with 2 steps

1: N,N-dimethyl-formamide / 0.5 h

2: copper(l) iodide; 1,10-Phenanthroline; potassium carbonate / N,N-dimethyl-formamide / 10 h / 110 °C / Inert atmosphere

With copper(l) iodide; 1,10-Phenanthroline; potassium carbonate; In N,N-dimethyl-formamide;
DOI:10.1016/j.tetlet.2014.01.006

Reference yield:

: 103-72-0
phenyl isothiocyanate

: 1564286-41-4
3-nitrophenyl N-bis(dimethylamino)methylene-N'-phenylcarbamimidothioate

Guidance literature:: Multi-step reaction with 2 steps

1: N,N-dimethyl-formamide / 0.5 h

2: copper(l) iodide; 1,10-Phenanthroline; potassium carbonate / N,N-dimethyl-formamide / 10 h / 110 °C / Inert atmosphere

With copper(l) iodide; 1,10-Phenanthroline; potassium carbonate; In N,N-dimethyl-formamide;
DOI:10.1016/j.tetlet.2014.01.006