(E)-4-(but-2-en-1-yl)-1-tosylpiperidine

Base Information

Chemical Name:(E)-4-(but-2-en-1-yl)-1-tosylpiperidine
CAS No.:1373334-64-5
Molecular Formula:C₁₆H₂₃NO₂S
Molecular Weight:293.43
Hs Code.:

Synonyms:(E)-4-(but-2-en-1-yl)-1-tosylpiperidine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (E)-4-(but-2-en-1-yl)-1-tosylpiperidine

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Technology Process of (E)-4-(but-2-en-1-yl)-1-tosylpiperidine

There total 4 articles about (E)-4-(but-2-en-1-yl)-1-tosylpiperidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 95151-35-2
3-buten-2-yl methyl carbonate

: 347885-68-1
4-bromo-1-tosylpiperidine

: 1373334-64-5
(E)-4-(but-2-en-1-yl)-1-tosylpiperidine

Guidance literature:: With bis(1,5-cyclooctadiene)nickel ⁽⁰⁾; magnesium chloride; 4,4',4-tri-tert-butyl-2,2':6',2-terpyridine; zinc; In N,N-dimethyl acetamide; at 80 ℃; for 12h; diastereoselective reaction; Inert atmosphere;
DOI:10.1002/chem.201102984

Reference yield: 88.0%

: 95151-35-2
3-buten-2-yl methyl carbonate

: 289890-80-8
4-iodo-1-[(4-methylphenyl)sulfonyl]piperidine

: 1373334-64-5
(E)-4-(but-2-en-1-yl)-1-tosylpiperidine

Guidance literature:: With bis(1,5-cyclooctadiene)nickel ⁽⁰⁾; copper(l) iodide; 2,6-bis((S)-4-isopropyl-4,5-dihydrooxazol-2-yl)pyridine; zinc; In N,N-dimethyl acetamide; at 35 ℃; for 6h; diastereoselective reaction; Inert atmosphere;
DOI:10.1002/chem.201102984

Reference yield: 82.0%

: 103185-13-3
(E)-crotyl methyl carbonate

: 347885-68-1
4-bromo-1-tosylpiperidine

: 1373334-64-5
(E)-4-(but-2-en-1-yl)-1-tosylpiperidine

Guidance literature:: With bis(1,5-cyclooctadiene)nickel ⁽⁰⁾; magnesium chloride; 4,4',4-tri-tert-butyl-2,2':6',2-terpyridine; zinc; In N,N-dimethyl acetamide; at 80 ℃; for 12h; Inert atmosphere;
DOI:10.1002/chem.201102984