benzylmethylamine of phthalimidocaproic acid

Base Information

Chemical Name:benzylmethylamine of phthalimidocaproic acid
CAS No.:195873-08-6
Molecular Formula:C₂₂H₂₄N₂O₃
Molecular Weight:364.444
Hs Code.:

Synonyms:benzylmethylamine of phthalimidocaproic acid

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Chemical Property of benzylmethylamine of phthalimidocaproic acid

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Technology Process of benzylmethylamine of phthalimidocaproic acid

There total 1 articles about benzylmethylamine of phthalimidocaproic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 4443-26-9
6-phthalimidohexanoic acid

: 100-46-9
benzylamine

: 195873-08-6
benzylmethylamine of phthalimidocaproic acid

Guidance literature:: With thionyl chloride; triethylamine; In benzene;
DOI:10.1007/BF02464118

Reference yield: 33.5%

: 195873-08-6
benzylmethylamine of phthalimidocaproic acid

: 195873-09-7
benzylmethylamine of aminocaproic acid

Guidance literature:: With hydrazine hydrate; In ethanol;
DOI:10.1007/BF02464118

Reference yield:

: 195873-08-6
benzylmethylamine of phthalimidocaproic acid

: N-benzyl-N'-(4-{[6-(benzyl-methyl-amino)-hexylamino]-methyl}-benzyl)-N-methyl-hexane-1,6-diamine

Guidance literature:: Multi-step reaction with 3 steps

1: 33.5 percent / hydrazine hydrate / ethanol

2: 91 percent / Et₃N / acetonitrile

3: 52 percent / LiAlH₄; NaOH / bis-(2-methoxy-ethyl) ether; ethanol / 5 h / 70 °C

With sodium hydroxide; lithium aluminium tetrahydride; hydrazine hydrate; triethylamine; In ethanol; diethylene glycol dimethyl ether; acetonitrile; 1: Decomposition / 2: Acylation / 3: Reduction;
DOI:10.1007/BF02464118