Technology Process of C30H26O3
There total 3 articles about C30H26O3 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
copper(l) iodide; tetrakis(triphenylphosphine) palladium(0); triethylamine;
In
diethyl ether;
at 20 ℃;
for 16h;
Inert atmosphere;
DOI:10.1039/c1ob06047c
- Guidance literature:
-
Multi-step reaction with 3 steps
1: copper(l) iodide; tetrakis(triphenylphosphine) palladium(0); triethylamine / N,N-dimethyl-formamide / 48 h / 70 °C / Inert atmosphere
2: potassium carbonate / methanol; dichloromethane / 3.5 h
3: copper(l) iodide; tetrakis(triphenylphosphine) palladium(0); triethylamine / diethyl ether / 16 h / 20 °C / Inert atmosphere
With
copper(l) iodide; tetrakis(triphenylphosphine) palladium(0); potassium carbonate; triethylamine;
In
methanol; diethyl ether; dichloromethane; N,N-dimethyl-formamide;
1: Sonogashira coupling / 3: Sonogashira coupling;
DOI:10.1039/c1ob06047c
- Guidance literature:
-
Multi-step reaction with 4 steps
1: copper(l) iodide; tetrakis(triphenylphosphine) palladium(0); triethylamine / tetrahydrofuran / 20 h / 20 °C / Inert atmosphere
2: copper(l) iodide; tetrakis(triphenylphosphine) palladium(0); triethylamine / N,N-dimethyl-formamide / 48 h / 70 °C / Inert atmosphere
3: potassium carbonate / methanol; dichloromethane / 3.5 h
4: copper(l) iodide; tetrakis(triphenylphosphine) palladium(0); triethylamine / diethyl ether / 16 h / 20 °C / Inert atmosphere
With
copper(l) iodide; tetrakis(triphenylphosphine) palladium(0); potassium carbonate; triethylamine;
In
tetrahydrofuran; methanol; diethyl ether; dichloromethane; N,N-dimethyl-formamide;
1: Sonogashira coupling / 2: Sonogashira coupling / 4: Sonogashira coupling;
DOI:10.1039/c1ob06047c