bis(diethylamino)-trimethylstannylethinylborane

Base Information

• Chemical Name: bis(diethylamino)-trimethylstannylethinylborane
• CAS No.: 109629-78-9
• Molecular Formula: C₁₃H₂₉BN₂Sn
• Molecular Weight: 342.908
• Mol file: 109629-78-9.mol

Synonyms:bis(diethylamino)-trimethylstannylethinylborane

Chemical Property of bis(diethylamino)-trimethylstannylethinylborane

Chemical Property:

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Technology Process of bis(diethylamino)-trimethylstannylethinylborane

There total 1 articles about bis(diethylamino)-trimethylstannylethinylborane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 35.0%

diethylamino-diethinylborane (62705-36-6) + Diethylamino-trimethyl-stannan (1068-74-2) → bis(diethylamino)-trimethylstannylethinylborane (109629-78-9) + diethylamino-bis(trimethylstannylethinyl)borane (109629-77-8) + bis(trimethyltin)acetylene (2117-50-2)

Guidance literature:

In neat (no solvent); byproducts: diethylamin; under N2; mixed at -78°C; warmed slowly to room temp. with stirring; heated slowly for 2 h up to 100°C; distd. (40 - 70°C, 1E-1 Torr); (Et2N)2BCCSnMe3 and Me3SnCCSnMe3 isolated; elem. anal.;

DOI:10.1016/0022-328X(86)80470-3

upstream raw materials:

diethylamino-diethinylborane

Diethylamino-trimethyl-stannan