N-{4-[4-(biphenyl-4-yl)-4-oxobutanamido]butyl}-5-(2,5-dimethylphenoxy)-2,2-dimethylpentanamide

Base Information

Chemical Name:N-{4-[4-(biphenyl-4-yl)-4-oxobutanamido]butyl}-5-(2,5-dimethylphenoxy)-2,2-dimethylpentanamide
CAS No.:1284259-13-7
Molecular Formula:C₃₅H₄₄N₂O₄
Molecular Weight:556.745
Hs Code.:

Synonyms:N-{4-[4-(biphenyl-4-yl)-4-oxobutanamido]butyl}-5-(2,5-dimethylphenoxy)-2,2-dimethylpentanamide

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Chemical Property of N-{4-[4-(biphenyl-4-yl)-4-oxobutanamido]butyl}-5-(2,5-dimethylphenoxy)-2,2-dimethylpentanamide

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Technology Process of N-{4-[4-(biphenyl-4-yl)-4-oxobutanamido]butyl}-5-(2,5-dimethylphenoxy)-2,2-dimethylpentanamide

There total 3 articles about N-{4-[4-(biphenyl-4-yl)-4-oxobutanamido]butyl}-5-(2,5-dimethylphenoxy)-2,2-dimethylpentanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 25812-30-0
gemfibrozil

: 1284258-79-2
N-(4-aminobutyl)-4-(biphenyl-4-yl)-4-oxobutanamide

: 1284259-13-7
N-{4-[4-(biphenyl-4-yl)-4-oxobutanamido]butyl}-5-(2,5-dimethylphenoxy)-2,2-dimethylpentanamide

Guidance literature:: With O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; for 0.25h; Inert atmosphere;
DOI:10.1016/j.bmcl.2011.01.068

Reference yield:

: 1284258-78-1
N-(4-azidobutyl)-4-(biphenyl-4-yl)-4-oxobutanamide

: 1284259-13-7
N-{4-[4-(biphenyl-4-yl)-4-oxobutanamido]butyl}-5-(2,5-dimethylphenoxy)-2,2-dimethylpentanamide

Guidance literature:: Multi-step reaction with 2 steps

1: 10% palladium on activated charcoal; hydrogen / methanol / 0.83 h

2: O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 0.25 h / Inert atmosphere

With 10% palladium on activated charcoal; hydrogen; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; In methanol; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2011.01.068

Reference yield:

: 36330-85-5
3-(p-phenyl)benzoylpropionic acid

: 1284259-13-7
N-{4-[4-(biphenyl-4-yl)-4-oxobutanamido]butyl}-5-(2,5-dimethylphenoxy)-2,2-dimethylpentanamide

Guidance literature:: Multi-step reaction with 3 steps

1: O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 1 h / Inert atmosphere

2: 10% palladium on activated charcoal; hydrogen / methanol / 0.83 h

3: O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 0.25 h / Inert atmosphere

With 10% palladium on activated charcoal; hydrogen; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; In methanol; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2011.01.068