Technology Process of C14H18O3
There total 8 articles about C14H18O3 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
triethylamine;
dmap;
In
dichloromethane;
at 0 - 20 ℃;
- Guidance literature:
-
δ-(4-methylphenyl)-δ-valerolactone;
With
diisobutylaluminium hydride;
In
dichloromethane;
at -78 ℃;
for 2h;
acetic anhydride;
With
triethylamine;
dmap;
In
dichloromethane;
at 0 - 20 ℃;
for 1h;
With
sodium hydrogencarbonate;
In
dichloromethane; water;
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: copper(I) bromide; lithium bromide / tetrahydrofuran / 18 h / 0 °C / Inert atmosphere
2.1: water; lithium hydroxide monohydrate / tetrahydrofuran / 1 h / 50 °C
2.2: pH 1
3.1: potassium hydroxide; sodium tetrahydroborate / water / 10 - 20 °C
4.1: trifluoroacetic acid / dichloromethane / 18 h / 20 °C
5.1: diisobutylaluminium hydride / dichloromethane / 2 h / -78 °C
5.2: -78 - 20 °C
6.1: triethylamine / dmap / dichloromethane / 0 - 20 °C
With
sodium tetrahydroborate; lithium hydroxide monohydrate; water; diisobutylaluminium hydride; triethylamine; trifluoroacetic acid; potassium hydroxide; copper(I) bromide; lithium bromide;
dmap;
In
tetrahydrofuran; dichloromethane; water;