4-N-(4-methoxyphenyl)-4-N,6-dimethyl-6,7-dihydro-5H-cyclopenta[d]pyrimidine-2,4-diamine

Base Information

Chemical Name:4-N-(4-methoxyphenyl)-4-N,6-dimethyl-6,7-dihydro-5H-cyclopenta[d]pyrimidine-2,4-diamine
CAS No.:1204408-21-8
Molecular Formula:C₁₆H₂₀N₄O
Molecular Weight:284.361
Hs Code.:

Synonyms:4-N-(4-methoxyphenyl)-4-N,6-dimethyl-6,7-dihydro-5H-cyclopenta[d]pyrimidine-2,4-diamine

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Chemical Property of 4-N-(4-methoxyphenyl)-4-N,6-dimethyl-6,7-dihydro-5H-cyclopenta[d]pyrimidine-2,4-diamine

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Technology Process of 4-N-(4-methoxyphenyl)-4-N,6-dimethyl-6,7-dihydro-5H-cyclopenta[d]pyrimidine-2,4-diamine

There total 3 articles about 4-N-(4-methoxyphenyl)-4-N,6-dimethyl-6,7-dihydro-5H-cyclopenta[d]pyrimidine-2,4-diamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 1204408-20-7
4-chloro-6-methyl-6,7-dihydro-5H-cyclopenta[d]pyrimidin-2-amine

: 5961-59-1
N-methyl-N-(4-methoxyphenyl)amine

: 1204408-21-8
4-N-(4-methoxyphenyl)-4-N,6-dimethyl-6,7-dihydro-5H-cyclopenta[d]pyrimidine-2,4-diamine

Guidance literature:: 4-chloro-6-methyl-6,7-dihydro-5H-cyclopenta[d]pyrimidin-2-amine; N-methyl-N-(4-methoxyphenyl)amine; With hydrogenchloride; water; In isopropyl alcohol; for 3h; Reflux;

With ammonium hydroxide; In water; Cooling with ice;

Reference yield:

: 3058-01-3,81177-02-8
3-methyladipic acid

: 1204408-21-8
4-N-(4-methoxyphenyl)-4-N,6-dimethyl-6,7-dihydro-5H-cyclopenta[d]pyrimidine-2,4-diamine

Guidance literature:: Multi-step reaction with 3 steps

1.1: sulfuric acid / ethanol / 8 h / Reflux

1.2: 3 h / Reflux

1.3: Reflux

2.1: trichlorophosphate / 3 h / Reflux

3.1: hydrogenchloride / isopropyl alcohol / Reflux

With hydrogenchloride; sulfuric acid; trichlorophosphate; In ethanol; isopropyl alcohol;
DOI:10.1021/jm400639z

Reference yield:

: 1204408-19-4
2-amino-6-methyl-3,5,6,7-tetrahydro-4H-cyclopenta[d]pyrimidin-4-one

: 1204408-21-8
4-N-(4-methoxyphenyl)-4-N,6-dimethyl-6,7-dihydro-5H-cyclopenta[d]pyrimidine-2,4-diamine

Guidance literature:: Multi-step reaction with 2 steps

1: trichlorophosphate / 3 h / Reflux

2: hydrogenchloride / isopropyl alcohol / Reflux

With hydrogenchloride; trichlorophosphate; In isopropyl alcohol;
DOI:10.1021/jm400639z