4-methyl phenyl 5-chloro-4-[3-chloro-4-(trifluoromethoxy)phenoxy]-2-fluorobenzoate

Base Information

Chemical Name:4-methyl phenyl 5-chloro-4-[3-chloro-4-(trifluoromethoxy)phenoxy]-2-fluorobenzoate
CAS No.:1354963-01-1
Molecular Formula:C₂₁H₁₂Cl₂F₄O₄
Molecular Weight:475.223
Hs Code.:

Synonyms:4-methyl phenyl 5-chloro-4-[3-chloro-4-(trifluoromethoxy)phenoxy]-2-fluorobenzoate

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Chemical Property of 4-methyl phenyl 5-chloro-4-[3-chloro-4-(trifluoromethoxy)phenoxy]-2-fluorobenzoate

Chemical Property:

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Technology Process of 4-methyl phenyl 5-chloro-4-[3-chloro-4-(trifluoromethoxy)phenoxy]-2-fluorobenzoate

There total 3 articles about 4-methyl phenyl 5-chloro-4-[3-chloro-4-(trifluoromethoxy)phenoxy]-2-fluorobenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 47.0%

: 1000339-94-5
3-chloro-4-(trifluoromethoxy)phenol

: 1354960-64-7
4-methylphenyl 5-chloro-2,4-difluorobenzoate

: 1354963-01-1
4-methyl phenyl 5-chloro-4-[3-chloro-4-(trifluoromethoxy)phenoxy]-2-fluorobenzoate

Guidance literature:: With potassium carbonate; In dimethyl sulfoxide; at 20 ℃; for 3h;

Reference yield:

: 5-chloro-2,4-difluorobenzoic acid

: 1354963-01-1
4-methyl phenyl 5-chloro-4-[3-chloro-4-(trifluoromethoxy)phenoxy]-2-fluorobenzoate

Guidance literature:: Multi-step reaction with 3 steps

1: thionyl chloride / 5 h / 60 °C / Inert atmosphere

2: triethylamine / dichloromethane / 16.16 h / 0 - 20 °C / Inert atmosphere

3: potassium carbonate / dimethyl sulfoxide / 3 h / 20 °C

With thionyl chloride; potassium carbonate; triethylamine; In dichloromethane; dimethyl sulfoxide;

Reference yield:

: 1261734-09-1
5-chloro-2,4-difluorobenzoyl chloride

: 1354963-01-1
4-methyl phenyl 5-chloro-4-[3-chloro-4-(trifluoromethoxy)phenoxy]-2-fluorobenzoate

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / dichloromethane / 16.16 h / 0 - 20 °C / Inert atmosphere

2: potassium carbonate / dimethyl sulfoxide / 3 h / 20 °C

With potassium carbonate; triethylamine; In dichloromethane; dimethyl sulfoxide;