C₁₇H₂₂O₅

Base Information

Chemical Name:C₁₇H₂₂O₅
CAS No.:1422042-42-9
Molecular Formula:C₁₇H₂₂O₅
Molecular Weight:306.359
Hs Code.:

C<sub>17</sub>H<sub>22</sub>O<sub>5</sub>

Synonyms:C₁₇H₂₂O₅

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₇H₂₂O₅

Chemical Property:

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Technology Process of C₁₇H₂₂O₅

There total 1 articles about C₁₇H₂₂O₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 2186-92-7
p-Anisaldehyde dimethyl acetal

: 1422042-41-8
C₉H₁₆O₄

: 1422042-42-9
C₁₇H₂₂O₅

Guidance literature:: With camphor-10-sulfonic acid; In dichloromethane; for 4h; Inert atmosphere;
DOI:10.1021/ol400014e

Reference yield: 92.0%

: 1422042-42-9
C₁₇H₂₂O₅

: 158673-92-8
(2S,3S)-3-(4-Methoxy-benzyloxy)-hept-6-ene-1,2-diol

Guidance literature:: With diisobutylaluminium hydride; In dichloromethane; toluene; at -78 - -13 ℃; for 120.25h; Inert atmosphere;
DOI:10.1021/ol400014e

Reference yield:

: 1422042-42-9
C₁₇H₂₂O₅

: C₅₈H₉₆O₈Si₂

Guidance literature:: Multi-step reaction with 11 steps

1.1: diisobutylaluminium hydride / dichloromethane; toluene / 120.25 h / -78 - -13 °C / Inert atmosphere

2.1: pyridine / dichloromethane / -78 °C / Inert atmosphere

3.1: 2,6-dimethylpyridine / dichloromethane / 1 h / 20 °C / Inert atmosphere

4.1: diisobutylaluminium hydride / dichloromethane; toluene / 1 h / -78 - 0 °C / Inert atmosphere

4.2: 2 h / 0 - 20 °C / Inert atmosphere

5.1: Dess-Martin periodane / dichloromethane; water / 1 h / 0 - 20 °C

6.1: barium hydroxide octahydrate / tetrahydrofuran; water / 20 °C / Inert atmosphere

7.1: sodium tetrahydroborate / methanol / 20 °C / Inert atmosphere

8.1: 2,6-dimethylpyridine / dichloromethane / 0.5 h / 20 °C / Inert atmosphere

9.1: potassium hydroxide / tetrahydrofuran; water / 12 h / 100 °C / Inert atmosphere

10.1: triethylamine; 2,4,6-trichlorobenzoyl chloride / toluene / 1 h / 20 °C / Inert atmosphere

10.2: 1 h / Inert atmosphere

11.1: triethylamine; caesium carbonate; palladium diacetate / N,N-dimethyl-formamide / 20 °C / Inert atmosphere

With pyridine; 2,6-dimethylpyridine; sodium tetrahydroborate; barium hydroxide octahydrate; 2,4,6-trichlorobenzoyl chloride; palladium diacetate; diisobutylaluminium hydride; caesium carbonate; Dess-Martin periodane; triethylamine; potassium hydroxide; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide; toluene; 5.1: |Dess-Martin Oxidation / 6.1: |Horner-Wadsworth-Emmons Olefination / 11.1: |Heck Reaction;
DOI:10.1021/ol400014e