(1-(12-(4-([2,2′,6′,2″-terpyridin]-4′-yl)phenyl)-2,9-dioctyl-1,3,8,10-tetraoxo-1,2,3,8,9,10-hexahydroanthra[2,1,9-def:6,5,10-d′e′f ′]diisoquinolin-5-yl)pyrrolidin-2-yl)methyl but-3-enoate

Base Information

Chemical Name:(1-(12-(4-([2,2′,6′,2″-terpyridin]-4′-yl)phenyl)-2,9-dioctyl-1,3,8,10-tetraoxo-1,2,3,8,9,10-hexahydroanthra[2,1,9-def:6,5,10-d′e′f ′]diisoquinolin-5-yl)pyrrolidin-2-yl)methyl but-3-enoate
CAS No.:1456722-74-9
Molecular Formula:C₇₀H₆₈N₆O₆
Molecular Weight:1089.35
Hs Code.:

(1-(12-(4-([2,2′,6′,2″-terpyridin]-4′-yl)phenyl)-2,9-dioctyl-1,3,8,10-tetraoxo-1,2,3,8,9,10-hexahydroanthra[2,1,9-def:6,5,10-d′e′f ′]diisoquinolin-5-yl)pyrrolidin-2-yl)methyl but-3-enoate

Synonyms:(1-(12-(4-([2,2′,6′,2″-terpyridin]-4′-yl)phenyl)-2,9-dioctyl-1,3,8,10-tetraoxo-1,2,3,8,9,10-hexahydroanthra[2,1,9-def:6,5,10-d′e′f ′]diisoquinolin-5-yl)pyrrolidin-2-yl)methyl but-3-enoate

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Chemical Property of (1-(12-(4-([2,2′,6′,2″-terpyridin]-4′-yl)phenyl)-2,9-dioctyl-1,3,8,10-tetraoxo-1,2,3,8,9,10-hexahydroanthra[2,1,9-def:6,5,10-d′e′f ′]diisoquinolin-5-yl)pyrrolidin-2-yl)methyl but-3-enoate

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Technology Process of (1-(12-(4-([2,2′,6′,2″-terpyridin]-4′-yl)phenyl)-2,9-dioctyl-1,3,8,10-tetraoxo-1,2,3,8,9,10-hexahydroanthra[2,1,9-def:6,5,10-d′e′f ′]diisoquinolin-5-yl)pyrrolidin-2-yl)methyl but-3-enoate

There total 1 articles about (1-(12-(4-([2,2′,6′,2″-terpyridin]-4′-yl)phenyl)-2,9-dioctyl-1,3,8,10-tetraoxo-1,2,3,8,9,10-hexahydroanthra[2,1,9-def:6,5,10-d′e′f ′]diisoquinolin-5-yl)pyrrolidin-2-yl)methyl but-3-enoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 625-38-7
but-3-enoic acid

: 1456722-70-5
5-(4-([2,2′,6′,2″-terpyridin]-4′-yl)phenyl)-12-(2-(hydroxymethyl)-pyrrolidin-1-yl)-2,9-dioctylanthra[2,1,9-def:6,5,10-d′e′f ′]diisoquinoline-1,3,8,10(2H,9H)tetraone

: 1456722-74-9
(1-(12-(4-([2,2′,6′,2″-terpyridin]-4′-yl)phenyl)-2,9-dioctyl-1,3,8,10-tetraoxo-1,2,3,8,9,10-hexahydroanthra[2,1,9-def:6,5,10-d′e′f ′]diisoquinolin-5-yl)pyrrolidin-2-yl)methyl but-3-enoate

Guidance literature:: With dmap; dicyclohexyl-carbodiimide; In dichloromethane; at 20 ℃; for 3.5h;
DOI:10.1039/c3ob41058g

Reference yield: 76.0%

: 24669-78-1
triethoxysilane

: 1456722-74-9
(1-(12-(4-([2,2′,6′,2″-terpyridin]-4′-yl)phenyl)-2,9-dioctyl-1,3,8,10-tetraoxo-1,2,3,8,9,10-hexahydroanthra[2,1,9-def:6,5,10-d′e′f ′]diisoquinolin-5-yl)pyrrolidin-2-yl)methyl but-3-enoate

: 1456722-76-1
(1-(12-(4-([2,2′,6′,2″-terpyridin]-4′-yl)phenyl)-2,9-dioctyl-1,3,8,10-tetraoxo-1,2,3,8,9,10-hexahydroanthra[2,1,9-def:6,5,10-d′e′f ′]diisoquinolin-5-yl)pyrrolidin-2-yl)methyl 4-(triethoxysilyl)butanoate

Guidance literature:: With platinum⁽⁰⁾-1,3-divinyl-1,1,3,3-tetramethyldisiloxane complex; In toluene; at 0 - 20 ℃; for 3h; Inert atmosphere; Sealed tube;
DOI:10.1039/c3ob41058g