threo-1-(mesitylsulfonyl)-2-[(4-mesitylsulfonylamino-1-phenylthio)butyl]pyrrolidine

Base Information

Chemical Name:threo-1-(mesitylsulfonyl)-2-[(4-mesitylsulfonylamino-1-phenylthio)butyl]pyrrolidine
CAS No.:1410797-77-1
Molecular Formula:C₃₂H₄₂N₂O₄S₃
Molecular Weight:614.894
Hs Code.:

Synonyms:threo-1-(mesitylsulfonyl)-2-[(4-mesitylsulfonylamino-1-phenylthio)butyl]pyrrolidine

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Chemical Property of threo-1-(mesitylsulfonyl)-2-[(4-mesitylsulfonylamino-1-phenylthio)butyl]pyrrolidine

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Technology Process of threo-1-(mesitylsulfonyl)-2-[(4-mesitylsulfonylamino-1-phenylthio)butyl]pyrrolidine

There total 10 articles about threo-1-(mesitylsulfonyl)-2-[(4-mesitylsulfonylamino-1-phenylthio)butyl]pyrrolidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₄H₃₃NO₅S₃

: 4543-58-2
2,4,6-trimethylbenzenesulfonamide

: 1410797-77-1
threo-1-(mesitylsulfonyl)-2-[(4-mesitylsulfonylamino-1-phenylthio)butyl]pyrrolidine

: C₃₂H₄₂N₂O₄S₃

Guidance literature:: 2,4,6-trimethylbenzenesulfonamide; With potassium hydroxide; In N,N-dimethyl-formamide; at 120 ℃; for 0.5h;

C₂₄H₃₃NO₅S₃; In N,N-dimethyl-formamide; at 120 ℃; for 5h; Overall yield = 1.07 g;
DOI:10.1016/j.tet.2012.08.043

Reference yield:

: C₂₃H₃₁NO₃S₂

: 1410797-77-1
threo-1-(mesitylsulfonyl)-2-[(4-mesitylsulfonylamino-1-phenylthio)butyl]pyrrolidine

: C₃₂H₄₂N₂O₄S₃

Guidance literature:: Multi-step reaction with 2 steps

1.1: triethylamine / tetrahydrofuran / 1.5 h / 0 - 20 °C

2.1: potassium hydroxide / N,N-dimethyl-formamide / 0.5 h / 120 °C

2.2: 5 h / 120 °C

With triethylamine; potassium hydroxide; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1016/j.tet.2012.08.043

Reference yield:

: C₂₅H₃₆O₄SSi

: 1410797-77-1
threo-1-(mesitylsulfonyl)-2-[(4-mesitylsulfonylamino-1-phenylthio)butyl]pyrrolidine

: C₃₂H₄₂N₂O₄S₃

Guidance literature:: Multi-step reaction with 7 steps

1.1: potassium hydroxide / N,N-dimethyl-formamide / 0.5 h / 120 °C

1.2: 5 h / 120 °C

2.1: oxone; tetra(n-butyl)ammonium hydrogensulfate; disodium ethylenediaminetetraacetic acid; potassium carbonate; acetic acid / acetonitrile / 0 °C

3.1: (1S)-10-camphorsulfonic acid / dichloromethane / 1.5 h / 25 °C

4.1: triethylamine / tetrahydrofuran / 3 h / 0 - 25 °C

5.1: tetrahydrofuran / 24 h / Reflux

5.2: 20 °C

6.1: triethylamine / tetrahydrofuran / 1.5 h / 0 - 20 °C

7.1: potassium hydroxide / N,N-dimethyl-formamide / 0.5 h / 120 °C

7.2: 5 h / 120 °C

With oxone; (1S)-10-camphorsulfonic acid; tetra(n-butyl)ammonium hydrogensulfate; disodium ethylenediaminetetraacetic acid; potassium carbonate; acetic acid; triethylamine; potassium hydroxide; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1016/j.tet.2012.08.043