N²-<3--N-<3-<(tert-butoxy)carbonylamino>propyl>amino>propanoyl>-N'-cyclohexylalaninamid

Base Information

• Chemical Name: N²-<3--N-<3-<(tert-butoxy)carbonylamino>propyl>amino>propanoyl>-N'-cyclohexylalaninamid
• CAS No.: 159360-34-6
• Molecular Formula: C₂₅H₄₆N₄O₆
• Molecular Weight: 498.663

Synonyms:N²-<3--N-<3-<(tert-butoxy)carbonylamino>propyl>amino>propanoyl>-N'-cyclohexylalaninamid

Chemical Property of N²-<3--N-<3-<(tert-butoxy)carbonylamino>propyl>amino>propanoyl>-N'-cyclohexylalaninamid

Chemical Property:

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Technology Process of N²-<3--N-<3-<(tert-butoxy)carbonylamino>propyl>amino>propanoyl>-N'-cyclohexylalaninamid

There total 6 articles about N²-<3--N-<3-<(tert-butoxy)carbonylamino>propyl>amino>propanoyl>-N'-cyclohexylalaninamid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N2-(benzyloxycarbonyl)-N1-cyclohexylalaninamid (17922-76-8) → N2-<3--N-<3-<(tert-butoxy)carbonylamino>propyl>amino>propanoyl>-N'-cyclohexylalaninamid (159360-34-6)

Guidance literature:

Multi-step reaction with 2 steps

1: hydrogen / 5percent Pd/C / methanol / 3 h

2: 1.) CDI / 1.) THF, 3 h, room temp., 2.) THF, 12 h

With hydrogen; 1,1'-carbonyldiimidazole; palladium on activated charcoal; In methanol;

DOI:10.1002/hlca.19940770408

Reference yield:

cyclohexylamine (108-91-8,157973-60-9) → N2-<3--N-<3-<(tert-butoxy)carbonylamino>propyl>amino>propanoyl>-N'-cyclohexylalaninamid (159360-34-6)

Guidance literature:

Multi-step reaction with 3 steps

1: 1.) ClCOOEt, Et₃N / 1.) THF, -15 deg C, 10 min, 2.) THF, 60 min, from -15 to 0 deg C

2: hydrogen / 5percent Pd/C / methanol / 3 h

3: 1.) CDI / 1.) THF, 3 h, room temp., 2.) THF, 12 h

With hydrogen; chloroformic acid ethyl ester; triethylamine; 1,1'-carbonyldiimidazole; palladium on activated charcoal; In methanol;

DOI:10.1002/hlca.19940770408

Reference yield:

di-tert-butyl dicarbonate (24424-99-5) → N2-<3--N-<3-<(tert-butoxy)carbonylamino>propyl>amino>propanoyl>-N'-cyclohexylalaninamid (159360-34-6)

Guidance literature:

Multi-step reaction with 3 steps

1: Et₃N / tetrahydrofuran / 12 h

2: 94 percent / NaOH / ethanol; H₂O / 4 h / Ambient temperature

3: 1.) CDI / 1.) THF, 3 h, room temp., 2.) THF, 12 h

With sodium hydroxide; triethylamine; 1,1'-carbonyldiimidazole; In tetrahydrofuran; ethanol; water;

DOI:10.1002/hlca.19940770408

upstream raw materials:

Alanin-cyclohexylamid

3--N-<3-<(tert-butoxy)carbonylamino>propyl>amino>propansaure

di-tert-butyl dicarbonate

N²-(benzyloxycarbonyl)-N¹-cyclohexylalaninamid

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