(S)-2-Benzyloxycarbonylamino-3-(4-hydroxy-3-iodo-phenyl)-propionic acid; compound with dicyclohexyl-amine

Base Information

Chemical Name:(S)-2-Benzyloxycarbonylamino-3-(4-hydroxy-3-iodo-phenyl)-propionic acid; compound with dicyclohexyl-amine
CAS No.:79677-64-8
Molecular Formula:C₁₂H₂₃N*C₁₇H₁₆INO₅
Molecular Weight:622.544
Hs Code.:

Synonyms:(S)-2-Benzyloxycarbonylamino-3-(4-hydroxy-3-iodo-phenyl)-propionic acid; compound with dicyclohexyl-amine

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Chemical Property of (S)-2-Benzyloxycarbonylamino-3-(4-hydroxy-3-iodo-phenyl)-propionic acid; compound with dicyclohexyl-amine

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Technology Process of (S)-2-Benzyloxycarbonylamino-3-(4-hydroxy-3-iodo-phenyl)-propionic acid; compound with dicyclohexyl-amine

There total 6 articles about (S)-2-Benzyloxycarbonylamino-3-(4-hydroxy-3-iodo-phenyl)-propionic acid; compound with dicyclohexyl-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 79677-62-6
(S)-2-(((benzyloxy)carbonyl)amino)-3-(4-hydroxy-3-iodophenyl)propanoic acid

: 101-83-7
N-cyclohexyl-cyclohexanamine

: 79677-64-8
(S)-2-Benzyloxycarbonylamino-3-(4-hydroxy-3-iodo-phenyl)-propionic acid; compound with dicyclohexyl-amine

Guidance literature:: In diethyl ether; at -5 ℃;
DOI:10.1002/jlac.198119810716

Reference yield:

: 19506-72-0
benzyl-8-quinolyl carbonate

: 79677-64-8
(S)-2-Benzyloxycarbonylamino-3-(4-hydroxy-3-iodo-phenyl)-propionic acid; compound with dicyclohexyl-amine

Guidance literature:: Multi-step reaction with 3 steps

1: 82 percent / pyridine / 23 h

2: 91 percent / 2N NaOH / acetone / 2 h / Ambient temperature

3: 97 percent / diethyl ether / -5 °C

With sodium hydroxide; In pyridine; diethyl ether; acetone;
DOI:10.1002/jlac.198119810716

Reference yield:

: 70-78-0
3-Iodo-L-tyrosine

: 79677-64-8
(S)-2-Benzyloxycarbonylamino-3-(4-hydroxy-3-iodo-phenyl)-propionic acid; compound with dicyclohexyl-amine

Guidance literature:: Multi-step reaction with 2 steps

1: 87 percent / 2 N NaOH / dimethylformamide / 1 h / 20 °C

2: 97 percent / diethyl ether / -5 °C

With sodium hydroxide; In diethyl ether; N,N-dimethyl-formamide;
DOI:10.1002/jlac.198119810716