N-[[2-(N-methyl)aminomethyl-4-t-butoxycarbonyl]phenyl]-L-aspartic acid β-methyl ester

Base Information

Chemical Name:N-[[2-(N-methyl)aminomethyl-4-t-butoxycarbonyl]phenyl]-L-aspartic acid β-methyl ester
CAS No.:171050-10-5
Molecular Formula:C₁₈H₂₆N₂O₆
Molecular Weight:366.414
Hs Code.:

Synonyms:N-[[2-(N-methyl)aminomethyl-4-t-butoxycarbonyl]phenyl]-L-aspartic acid β-methyl ester

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Chemical Property of N-[[2-(N-methyl)aminomethyl-4-t-butoxycarbonyl]phenyl]-L-aspartic acid β-methyl ester

Chemical Property:

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Technology Process of N-[[2-(N-methyl)aminomethyl-4-t-butoxycarbonyl]phenyl]-L-aspartic acid β-methyl ester

There total 6 articles about N-[[2-(N-methyl)aminomethyl-4-t-butoxycarbonyl]phenyl]-L-aspartic acid β-methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 171050-09-2
N-[[2-formyl-4-t-butoxycarbonyl]phenyl]-L-aspartic acid β-methyl ester

: 171050-10-5
N-[[2-(N-methyl)aminomethyl-4-t-butoxycarbonyl]phenyl]-L-aspartic acid β-methyl ester

Guidance literature:: With magnesium sulfate; acetic acid; methylamine; In methanol; dichloromethane; water; ethyl acetate; acetonitrile;

Reference yield:

: (S)-2-{4-tert-Butoxycarbonyl-2-[(E)-methyliminomethyl]-phenylamino}-succinic acid 4-methyl ester

: 171050-10-5
N-[[2-(N-methyl)aminomethyl-4-t-butoxycarbonyl]phenyl]-L-aspartic acid β-methyl ester

Guidance literature:: With hydrogen; platinum(IV) oxide; In acetic acid;
DOI:10.1016/S0040-4039(97)00570-4

Reference yield:

: 2177-62-0
β-methyl L-aspartate

: 171050-10-5
N-[[2-(N-methyl)aminomethyl-4-t-butoxycarbonyl]phenyl]-L-aspartic acid β-methyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 75 percent / NaHCO₃ / dimethylsulfoxide; H₂O / 24 h / 72 °C

2: 84 percent / pyridine, HOAc, H₂O, H₂ / Raney/Ni / 60 °C

3: MgSO₄ / ethyl acetate

4: H₂ / PtO₂ / acetic acid

With pyridine; water; hydrogen; sodium hydrogencarbonate; magnesium sulfate; acetic acid; platinum(IV) oxide; Raney/Ni; In water; acetic acid; dimethyl sulfoxide; ethyl acetate;
DOI:10.1016/S0040-4039(97)00570-4