(5S,8R,9R)-10-Methyl-8,9-bis(benzoyloxy)-4,7-dioxo-5-methyl-3,6-diazadecanedicarboxylate

Base Information

Chemical Name:(5S,8R,9R)-10-Methyl-8,9-bis(benzoyloxy)-4,7-dioxo-5-methyl-3,6-diazadecanedicarboxylate
CAS No.:263550-09-0
Molecular Formula:C₂₄H₂₄N₂O₁₀
Molecular Weight:500.462
Hs Code.:

Synonyms:(5S,8R,9R)-10-Methyl-8,9-bis(benzoyloxy)-4,7-dioxo-5-methyl-3,6-diazadecanedicarboxylate

Suppliers and Price of (5S,8R,9R)-10-Methyl-8,9-bis(benzoyloxy)-4,7-dioxo-5-methyl-3,6-diazadecanedicarboxylate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (5S,8R,9R)-10-Methyl-8,9-bis(benzoyloxy)-4,7-dioxo-5-methyl-3,6-diazadecanedicarboxylate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (5S,8R,9R)-10-Methyl-8,9-bis(benzoyloxy)-4,7-dioxo-5-methyl-3,6-diazadecanedicarboxylate

There total 3 articles about (5S,8R,9R)-10-Methyl-8,9-bis(benzoyloxy)-4,7-dioxo-5-methyl-3,6-diazadecanedicarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 263550-06-7
(5S,8R,9R)-1-Benzyl-10-methyl-8,9-bis(benzoyloxy)-4,7-dioxo-5-methyl-3,6-diazadecanedicarboxylate

: 263550-09-0
(5S,8R,9R)-10-Methyl-8,9-bis(benzoyloxy)-4,7-dioxo-5-methyl-3,6-diazadecanedicarboxylate

Guidance literature:: With hydrogen; palladium on activated charcoal; In 1,4-dioxane;
DOI:10.1002/(SICI)1521-3765(20000117)6:2<247::AID-CHEM247>3.0.CO;2-M

Reference yield:

: 115061-55-7
(2R,3R)-2,3-dibenzoyloxy-3-methoxycarbonylpropanoic acid

: 263550-09-0
(5S,8R,9R)-10-Methyl-8,9-bis(benzoyloxy)-4,7-dioxo-5-methyl-3,6-diazadecanedicarboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: 58 percent / DCC; Et₃N / CH₂Cl₂ / 0 - 20 °C

2: 100 percent / H₂ / 10 percent Pd/C / dioxane

With hydrogen; triethylamine; dicyclohexyl-carbodiimide; palladium on activated charcoal; In 1,4-dioxane; dichloromethane; 1: Acylation / 2: Hydrogenolysis;
DOI:10.1002/(SICI)1521-3765(20000117)6:2<247::AID-CHEM247>3.0.CO;2-M

Reference yield:

: ((S)-2-Amino-propionylamino)-acetic acid benzyl ester; hydrobromide

: 263550-09-0
(5S,8R,9R)-10-Methyl-8,9-bis(benzoyloxy)-4,7-dioxo-5-methyl-3,6-diazadecanedicarboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: 58 percent / DCC; Et₃N / CH₂Cl₂ / 0 - 20 °C

2: 100 percent / H₂ / 10 percent Pd/C / dioxane

With hydrogen; triethylamine; dicyclohexyl-carbodiimide; palladium on activated charcoal; In 1,4-dioxane; dichloromethane; 1: Acylation / 2: Hydrogenolysis;
DOI:10.1002/(SICI)1521-3765(20000117)6:2<247::AID-CHEM247>3.0.CO;2-M