2'-(trisisopropylsiloxy)methyl-5'-(4,4'-dimethoxytrityl)-5-methoxyquinazoline-2,4-(1H,3H)-dione ribonucleoside

Base Information

Chemical Name:2'-(trisisopropylsiloxy)methyl-5'-(4,4'-dimethoxytrityl)-5-methoxyquinazoline-2,4-(1H,3H)-dione ribonucleoside
CAS No.:1199886-97-9
Molecular Formula:C₄₅H₅₆N₂O₁₀Si
Molecular Weight:813.033
Hs Code.:

Synonyms:2'-(trisisopropylsiloxy)methyl-5'-(4,4'-dimethoxytrityl)-5-methoxyquinazoline-2,4-(1H,3H)-dione ribonucleoside

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Chemical Property of 2'-(trisisopropylsiloxy)methyl-5'-(4,4'-dimethoxytrityl)-5-methoxyquinazoline-2,4-(1H,3H)-dione ribonucleoside

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Technology Process of 2'-(trisisopropylsiloxy)methyl-5'-(4,4'-dimethoxytrityl)-5-methoxyquinazoline-2,4-(1H,3H)-dione ribonucleoside

There total 1 articles about 2'-(trisisopropylsiloxy)methyl-5'-(4,4'-dimethoxytrityl)-5-methoxyquinazoline-2,4-(1H,3H)-dione ribonucleoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 30.0%

: 1199886-94-6
5'-(4,4'-dimethoxytrityl)-5-methoxyquinazoline-2,4-(1H,3H)-dione ribonucleoside

: 217300-17-9
chloromethoxy-triisopropyl-silane

: 1199886-97-9
2'-(trisisopropylsiloxy)methyl-5'-(4,4'-dimethoxytrityl)-5-methoxyquinazoline-2,4-(1H,3H)-dione ribonucleoside

Guidance literature:: 5'-(4,4'-dimethoxytrityl)-5-methoxyquinazoline-2,4-(1H,3H)-dione ribonucleoside; With dibutyltin chloride; N-ethyl-N,N-diisopropylamine; In 1,2-dichloro-ethane; at 20 - 80 ℃; for 1.16667h;

chloromethoxy-triisopropyl-silane; In 1,2-dichloro-ethane; at 80 ℃; for 0.25h;
DOI:10.1021/ja905767g