2-(2-bromo-4,5-dimethoxyphenyl)-1-(6-vinylbenzo[d][1,3]dioxol-5-yl)ethanone

Base Information

Chemical Name:2-(2-bromo-4,5-dimethoxyphenyl)-1-(6-vinylbenzo[d][1,3]dioxol-5-yl)ethanone
CAS No.:1252584-50-1
Molecular Formula:C₁₉H₁₇BrO₅
Molecular Weight:405.245
Hs Code.:

Synonyms:2-(2-bromo-4,5-dimethoxyphenyl)-1-(6-vinylbenzo[d][1,3]dioxol-5-yl)ethanone

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Chemical Property of 2-(2-bromo-4,5-dimethoxyphenyl)-1-(6-vinylbenzo[d][1,3]dioxol-5-yl)ethanone

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Technology Process of 2-(2-bromo-4,5-dimethoxyphenyl)-1-(6-vinylbenzo[d][1,3]dioxol-5-yl)ethanone

There total 1 articles about 2-(2-bromo-4,5-dimethoxyphenyl)-1-(6-vinylbenzo[d][1,3]dioxol-5-yl)ethanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2-(6-bromobenzo[d][1,3]dioxol-5-yl)-2-(trimethylsilyloxy)acetonitrile

: 53207-00-4
1-bromo-2-(bromomethyl)-4,5-dimethoxybenzene

: 1252584-50-1
2-(2-bromo-4,5-dimethoxyphenyl)-1-(6-vinylbenzo[d][1,3]dioxol-5-yl)ethanone

Guidance literature:: 2-(6-bromobenzo[d][1,3]dioxol-5-yl)-2-(trimethylsilyloxy)acetonitrile; With lithium hexamethyldisilazane; In tetrahydrofuran; at -78 ℃; for 1.16667h; Inert atmosphere;

1-bromo-2-(bromomethyl)-4,5-dimethoxybenzene; In tetrahydrofuran; at -78 - 10 ℃; Inert atmosphere;

With water; sodium hydroxide; In tetrahydrofuran; for 2h; Inert atmosphere;
DOI:10.1002/chem.201001689

Reference yield: 60.0%

: 1252584-50-1
2-(2-bromo-4,5-dimethoxyphenyl)-1-(6-vinylbenzo[d][1,3]dioxol-5-yl)ethanone

: 62-53-3
aniline

: 1252584-51-2
N-(2-(2-bromo-4,5-dimethoxyphenyl)-1-(6-vinylbenzo[d][1,3]dioxol-5-yl)ethyl)aniline

Guidance literature:: 2-(2-bromo-4,5-dimethoxyphenyl)-1-(6-vinylbenzo[d][1,3]dioxol-5-yl)ethanone; aniline; With titanium tetrachloride; triethylamine; In 1,2-dimethoxyethane; dichloromethane; at -78 - 50 ℃; Inert atmosphere;

With sodium cyanoborohydride; In methanol; 1,2-dimethoxyethane; dichloromethane; at 20 ℃; for 20h; Inert atmosphere;
DOI:10.1002/chem.201001689

Reference yield: 42.0%

: 1252584-50-1
2-(2-bromo-4,5-dimethoxyphenyl)-1-(6-vinylbenzo[d][1,3]dioxol-5-yl)ethanone

: 100-46-9
benzylamine

: 1252584-52-3
N-benzyl-2-(2-bromo-4,5-dimethoxyphenyl)-1-(6-vinylbenzo[d][1,3]dioxol-5-yl)ethanamine

Guidance literature:: 2-(2-bromo-4,5-dimethoxyphenyl)-1-(6-vinylbenzo[d][1,3]dioxol-5-yl)ethanone; benzylamine; With titanium tetrachloride; triethylamine; In 1,2-dimethoxyethane; dichloromethane; at -78 - 50 ℃; Inert atmosphere;

With sodium cyanoborohydride; In methanol; 1,2-dimethoxyethane; dichloromethane; at 20 ℃; for 10h; Inert atmosphere;
DOI:10.1002/chem.201001689