7-Methoxy-1,1,4-tris-(4-methoxy-phenyl)-1,2,3,4-tetrahydro-naphthalene

Base Information

• Chemical Name: 7-Methoxy-1,1,4-tris-(4-methoxy-phenyl)-1,2,3,4-tetrahydro-naphthalene
• CAS No.: 104267-17-6
• Molecular Formula: C₃₂H₃₂O₄
• Molecular Weight: 480.604
• Mol file: 104267-17-6.mol

Synonyms:7-Methoxy-1,1,4-tris-(4-methoxy-phenyl)-1,2,3,4-tetrahydro-naphthalene

Chemical Property of 7-Methoxy-1,1,4-tris-(4-methoxy-phenyl)-1,2,3,4-tetrahydro-naphthalene

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of 7-Methoxy-1,1,4-tris-(4-methoxy-phenyl)-1,2,3,4-tetrahydro-naphthalene

There total 2 articles about 7-Methoxy-1,1,4-tris-(4-methoxy-phenyl)-1,2,3,4-tetrahydro-naphthalene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1,1-bis-(4-methoxyphenyl)ethylene (4356-69-8) → 7-Methoxy-1,1,4-tris-(4-methoxy-phenyl)-1,2-dihydro-naphthalene (104267-18-7) + 7-Methoxy-1,1,4-tris-(4-methoxy-phenyl)-1,2,3,4-tetrahydro-naphthalene (104267-17-6)

Guidance literature:

With 2,6,9,10-tetracyanoanthracene; In acetonitrile; for 48h; Irradiation;

DOI:10.1021/ja00283a034

Reference yield:

1,1-bis-(4-methoxyphenyl)ethylene (4356-69-8) → 1,1,4,4-tetrakis(4-methoxyphenyl)butadiene (54655-89-9) + 1,1,3,3-Tetrakis-p-methoxyphenylbut-1-en (39117-63-0) + 7-Methoxy-1,1,4-tris-(4-methoxy-phenyl)-1,2-dihydro-naphthalene (104267-18-7) + 1,1,4,4-tetraanisyl-1-butene (110173-90-5) + 7-Methoxy-1,1,4-tris-(4-methoxy-phenyl)-1,2,3,4-tetrahydro-naphthalene (104267-17-6) + 2,2,3,3-tetrakis(4-methoxyphenyl)butane (110173-91-6)

Guidance literature:

With cadmium(II) sulphide; In dichloromethane; for 2h; Product distribution; Mechanism; Irradiation; other reagents and reaction times; also for reaction in the presence of O₂;

DOI:10.1021/jo00230a019

upstream raw materials:

1,1-bis-(4-methoxyphenyl)ethylene