C₁₂H₁₅BrO₄

Base Information

Chemical Name:C₁₂H₁₅BrO₄
CAS No.:1571072-99-5
Molecular Formula:C₁₂H₁₅BrO₄
Molecular Weight:303.153
Hs Code.:

C<sub>12</sub>H<sub>15</sub>BrO<sub>4</sub>

Synonyms:C₁₂H₁₅BrO₄

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Chemical Property of C₁₂H₁₅BrO₄

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Technology Process of C₁₂H₁₅BrO₄

There total 4 articles about C₁₂H₁₅BrO₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 1571073-00-1
C₁₂H₁₃BrO₄

: 1571072-99-5
C₁₂H₁₅BrO₄

Guidance literature:: With sodium tris(acetoxy)borohydride; In acetic acid; acetonitrile; at 0 ℃; for 1h; Inert atmosphere;
DOI:10.1021/jo4028227

Reference yield:

: 791642-68-7
4-bromo-1-iodo-2-methoxybenzene

: 1571072-99-5
C₁₂H₁₅BrO₄

Guidance literature:: Multi-step reaction with 3 steps

1: tributyl-amine; palladium diacetate; triphenyl-arsane / N,N-dimethyl-formamide / 15 h / 70 °C / Inert atmosphere

2: tetrabutyl ammonium fluoride / N,N-dimethyl-formamide; tetrahydrofuran / 1.5 h / 0 °C / Inert atmosphere

3: sodium tris(acetoxy)borohydride / acetic acid; acetonitrile / 1 h / 0 °C / Inert atmosphere

With tributyl-amine; triphenyl-arsane; tetrabutyl ammonium fluoride; palladium diacetate; sodium tris(acetoxy)borohydride; In tetrahydrofuran; acetic acid; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1021/jo4028227

Reference yield:

: C₂₄H₄₃BrO₄Si₂

: 1571072-99-5
C₁₂H₁₅BrO₄

Guidance literature:: Multi-step reaction with 2 steps

1: tetrabutyl ammonium fluoride / N,N-dimethyl-formamide; tetrahydrofuran / 1.5 h / 0 °C / Inert atmosphere

2: sodium tris(acetoxy)borohydride / acetic acid; acetonitrile / 1 h / 0 °C / Inert atmosphere

With tetrabutyl ammonium fluoride; sodium tris(acetoxy)borohydride; In tetrahydrofuran; acetic acid; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1021/jo4028227