methyl 4-<2-<5-<<(cyclopentyloxy)carbonyl>amino>-2-(methylamino)phenyl>-2-oxoethyl>-3-methoxybenzoate

Base Information

Chemical Name:methyl 4-<2-<5-<<(cyclopentyloxy)carbonyl>amino>-2-(methylamino)phenyl>-2-oxoethyl>-3-methoxybenzoate
CAS No.:127973-92-6
Molecular Formula:C₂₄H₂₈N₂O₆
Molecular Weight:440.496
Hs Code.:

Synonyms:methyl 4-<2-<5-<<(cyclopentyloxy)carbonyl>amino>-2-(methylamino)phenyl>-2-oxoethyl>-3-methoxybenzoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl 4-<2-<5-<<(cyclopentyloxy)carbonyl>amino>-2-(methylamino)phenyl>-2-oxoethyl>-3-methoxybenzoate

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Technology Process of methyl 4-<2-<5-<<(cyclopentyloxy)carbonyl>amino>-2-(methylamino)phenyl>-2-oxoethyl>-3-methoxybenzoate

There total 1 articles about methyl 4-<2-<5-<<(cyclopentyloxy)carbonyl>amino>-2-(methylamino)phenyl>-2-oxoethyl>-3-methoxybenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 107786-92-5
methyl 4-<2-<5-<<(cyclopentyloxy)carbonyl>amino>-2-(N-formyl-N-methylamino)phenyl>-2-oxoethyl>-3-methoxybenzoate

: 127973-92-6
methyl 4-<2-<5-<<(cyclopentyloxy)carbonyl>amino>-2-(methylamino)phenyl>-2-oxoethyl>-3-methoxybenzoate

Guidance literature:: With hydrogenchloride; In methanol; for 80h; Heating;
DOI:10.1021/jm00171a043

Reference yield: 62.0%

: 127973-92-6
methyl 4-<2-<5-<<(cyclopentyloxy)carbonyl>amino>-2-(methylamino)phenyl>-2-oxoethyl>-3-methoxybenzoate

: 127973-93-7
4-<2-<5-<<(cyclopentyloxy)carbonyl>amino>-2-(methylamino)phenyl>-2-oxoethyl>-3-methoxybenzoic acid

Guidance literature:: With lithium hydroxide; In tetrahydrofuran; methanol; for 4h;
DOI:10.1021/jm00171a043

Reference yield:

: 127973-92-6
methyl 4-<2-<5-<<(cyclopentyloxy)carbonyl>amino>-2-(methylamino)phenyl>-2-oxoethyl>-3-methoxybenzoate

: 127973-94-8
(3-{2-[2-Methoxy-4-(toluene-2-sulfonylaminocarbonyl)-phenyl]-acetyl}-4-methylamino-phenyl)-carbamic acid cyclopentyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 62 percent / aq. LiOH / tetrahydrofuran; methanol / 4 h

2: 48 percent / 1-<3-(dimethylamino)propyl>-3-ethylcarbodiimide hydrochloride, 4-(dimethylamino)pyridine / CH₂Cl₂ / 48 h

With dmap; lithium hydroxide; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1021/jm00171a043