5-{(E)-2-[3,5-dimethoxy-4-(methoxymetoxy)phenyl]vinyl}-1,3-dimethyl-2-nitrobenzene

Base Information

Chemical Name:5-{(E)-2-[3,5-dimethoxy-4-(methoxymetoxy)phenyl]vinyl}-1,3-dimethyl-2-nitrobenzene
CAS No.:1313376-42-9
Molecular Formula:C₂₀H₂₃NO₆
Molecular Weight:373.406
Hs Code.:

Synonyms:5-{(E)-2-[3,5-dimethoxy-4-(methoxymetoxy)phenyl]vinyl}-1,3-dimethyl-2-nitrobenzene

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Chemical Property of 5-{(E)-2-[3,5-dimethoxy-4-(methoxymetoxy)phenyl]vinyl}-1,3-dimethyl-2-nitrobenzene

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Technology Process of 5-{(E)-2-[3,5-dimethoxy-4-(methoxymetoxy)phenyl]vinyl}-1,3-dimethyl-2-nitrobenzene

There total 5 articles about 5-{(E)-2-[3,5-dimethoxy-4-(methoxymetoxy)phenyl]vinyl}-1,3-dimethyl-2-nitrobenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 864513-22-4
diethyl (3,5-dimethyl-4-nitrobenzyl)phosphonate

: 55211-66-0
3,5-dimethoxy-4-(methoxymethoxy)benzaldehyde

: 1313376-42-9
5-{(E)-2-[3,5-dimethoxy-4-(methoxymetoxy)phenyl]vinyl}-1,3-dimethyl-2-nitrobenzene

Guidance literature:: diethyl (3,5-dimethyl-4-nitrobenzyl)phosphonate; With sodium hydride; In tetrahydrofuran; mineral oil; at 20 ℃; for 0.25h;

3,5-dimethoxy-4-(methoxymethoxy)benzaldehyde; In tetrahydrofuran; mineral oil; at 20 ℃; for 5h;
DOI:10.1039/c1cc11681a

Reference yield:

: 18515-22-5
(3,5-dimethyl-4-nitrophenyl)methanol

: 1313376-42-9
5-{(E)-2-[3,5-dimethoxy-4-(methoxymetoxy)phenyl]vinyl}-1,3-dimethyl-2-nitrobenzene

Guidance literature:: Multi-step reaction with 3 steps

1.1: phosphorus tribromide / 2 h / 20 °C

2.1: tetra-(n-butyl)ammonium iodide / 4.5 h / 120 °C

3.1: sodium hydride / tetrahydrofuran; mineral oil / 0.25 h / 20 °C

3.2: 5 h / 20 °C

With phosphorus tribromide; tetra-(n-butyl)ammonium iodide; sodium hydride; In tetrahydrofuran; mineral oil;
DOI:10.1039/c1cc11681a

Reference yield:

: 40113-65-3
5-(bromomethyl)-1,3-dimethyl-2-nitrobenzene

: 1313376-42-9
5-{(E)-2-[3,5-dimethoxy-4-(methoxymetoxy)phenyl]vinyl}-1,3-dimethyl-2-nitrobenzene

Guidance literature:: Multi-step reaction with 2 steps

1.1: tetra-(n-butyl)ammonium iodide / 4.5 h / 120 °C

2.1: sodium hydride / tetrahydrofuran; mineral oil / 0.25 h / 20 °C

2.2: 5 h / 20 °C

With tetra-(n-butyl)ammonium iodide; sodium hydride; In tetrahydrofuran; mineral oil;
DOI:10.1039/c1cc11681a