ethyl 4-<(E)-2-nitroethenyl>phenyl glutarate

Base Information

Chemical Name:ethyl 4-<(E)-2-nitroethenyl>phenyl glutarate
CAS No.:142728-07-2
Molecular Formula:C₁₅H₁₇NO₆
Molecular Weight:307.303
Hs Code.:

Synonyms:ethyl 4-<(E)-2-nitroethenyl>phenyl glutarate

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Chemical Property of ethyl 4-<(E)-2-nitroethenyl>phenyl glutarate

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Technology Process of ethyl 4-<(E)-2-nitroethenyl>phenyl glutarate

There total 2 articles about ethyl 4-<(E)-2-nitroethenyl>phenyl glutarate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 5205-39-0
ethyl glutaroyl chloride

: 22568-49-6
(E)-1-(4-hydroxyphenyl)-2-nitroethene

: 142728-07-2
ethyl 4-<(E)-2-nitroethenyl>phenyl glutarate

Guidance literature:: With trifluorormethanesulfonic acid; In dichloromethane; for 6.5h; Ambient temperature;
DOI:10.1002/hlca.19920750304

Reference yield:

: 123-08-0,65581-83-1
4-hydroxy-benzaldehyde

: 142728-07-2
ethyl 4-<(E)-2-nitroethenyl>phenyl glutarate

Guidance literature:: Multi-step reaction with 2 steps

1: 69 percent / aniline / 6 h / 80 °C

2: 80 percent / trifluoromethanesulfonic acid / CH₂Cl₂ / 6.5 h / Ambient temperature

With trifluorormethanesulfonic acid; aniline; In dichloromethane;
DOI:10.1002/hlca.19920750304