2-[(2-bromo-5-methoxybenzyl)(toluene-4-sulfonyl)amino]-3-phenylpropionic acid methyl ester

Base Information

Chemical Name:2-[(2-bromo-5-methoxybenzyl)(toluene-4-sulfonyl)amino]-3-phenylpropionic acid methyl ester
CAS No.:1303530-15-5
Molecular Formula:C₂₅H₂₆BrNO₅S
Molecular Weight:532.455
Hs Code.:

Synonyms:2-[(2-bromo-5-methoxybenzyl)(toluene-4-sulfonyl)amino]-3-phenylpropionic acid methyl ester

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Chemical Property of 2-[(2-bromo-5-methoxybenzyl)(toluene-4-sulfonyl)amino]-3-phenylpropionic acid methyl ester

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Technology Process of 2-[(2-bromo-5-methoxybenzyl)(toluene-4-sulfonyl)amino]-3-phenylpropionic acid methyl ester

There total 3 articles about 2-[(2-bromo-5-methoxybenzyl)(toluene-4-sulfonyl)amino]-3-phenylpropionic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 19614-12-1
2-bromo-5-methoxybenzyl bromide

: 51220-86-1,149703-21-9,42384-33-8
N-(p-toluenesulfonyl)-L-phenylalanine methyl ester

: 1303530-15-5
2-[(2-bromo-5-methoxybenzyl)(toluene-4-sulfonyl)amino]-3-phenylpropionic acid methyl ester

Guidance literature:: N-(p-toluenesulfonyl)-L-phenylalanine methyl ester; With potassium carbonate; In acetonitrile; at 25 ℃; for 0.5h; Sonication;

2-bromo-5-methoxybenzyl bromide; In acetonitrile; at 25 ℃; for 14h; Sonication;
DOI:10.1055/s-0030-1258406

Reference yield:

: 63-91-2,25191-15-5,658-69-5,67675-33-6
L-phenylalanine

: 1303530-15-5
2-[(2-bromo-5-methoxybenzyl)(toluene-4-sulfonyl)amino]-3-phenylpropionic acid methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydroxide / water / 25 °C

2.1: toluene-4-sulfonic acid / 20 h / 90 °C

3.1: potassium carbonate / acetonitrile / 0.5 h / 25 °C / Sonication

3.2: 14 h / 25 °C / Sonication

With potassium carbonate; toluene-4-sulfonic acid; sodium hydroxide; In water; acetonitrile;
DOI:10.1055/s-0030-1258406

Reference yield:

: 98-59-9
p-toluenesulfonyl chloride

: 1303530-15-5
2-[(2-bromo-5-methoxybenzyl)(toluene-4-sulfonyl)amino]-3-phenylpropionic acid methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydroxide / water / 25 °C

2.1: toluene-4-sulfonic acid / 20 h / 90 °C

3.1: potassium carbonate / acetonitrile / 0.5 h / 25 °C / Sonication

3.2: 14 h / 25 °C / Sonication

With potassium carbonate; toluene-4-sulfonic acid; sodium hydroxide; In water; acetonitrile;
DOI:10.1055/s-0030-1258406