Technology Process of C25H24N6O5
There total 9 articles about C25H24N6O5 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
tetrabutyl ammonium fluoride;
In
dichloromethane;
at 20 ℃;
for 5h;
DOI:10.1039/c4ob00923a
- Guidance literature:
-
Multi-step reaction with 10 steps
1: sulfuric acid; nitric acid / 0.33 h
2: chromium(VI) oxide; acetic acid / Reflux
3: sulfuric acid / Reflux
4: N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile) / tetrachloromethane / Reflux
5: silver(II) sulfate / water / 3 h / Reflux
6: zinc; acetic acid / dichloromethane; acetonitrile / 5 h / 20 °C
7: hydrogenchloride; sodium nitrite; sodium azide / water / 20 °C / Reflux
8: 1H-imidazole / dichloromethane / 3 h / 20 °C
9: dicyclohexyl-carbodiimide; dmap / dichloromethane / 0 °C / Inert atmosphere
10: tetrabutyl ammonium fluoride / dichloromethane / 5 h / 20 °C
With
1H-imidazole; hydrogenchloride; dmap; N-Bromosuccinimide; sodium azide; silver(II) sulfate; 2,2'-azobis(isobutyronitrile); sulfuric acid; tetrabutyl ammonium fluoride; nitric acid; chromium(VI) oxide; acetic acid; dicyclohexyl-carbodiimide; zinc; sodium nitrite;
In
tetrachloromethane; dichloromethane; water; acetonitrile;
DOI:10.1039/c4ob00923a
- Guidance literature:
-
Multi-step reaction with 9 steps
1: chromium(VI) oxide; acetic acid / Reflux
2: sulfuric acid / Reflux
3: N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile) / tetrachloromethane / Reflux
4: silver(II) sulfate / water / 3 h / Reflux
5: zinc; acetic acid / dichloromethane; acetonitrile / 5 h / 20 °C
6: hydrogenchloride; sodium nitrite; sodium azide / water / 20 °C / Reflux
7: 1H-imidazole / dichloromethane / 3 h / 20 °C
8: dicyclohexyl-carbodiimide; dmap / dichloromethane / 0 °C / Inert atmosphere
9: tetrabutyl ammonium fluoride / dichloromethane / 5 h / 20 °C
With
1H-imidazole; hydrogenchloride; dmap; N-Bromosuccinimide; sodium azide; silver(II) sulfate; 2,2'-azobis(isobutyronitrile); sulfuric acid; tetrabutyl ammonium fluoride; chromium(VI) oxide; acetic acid; dicyclohexyl-carbodiimide; zinc; sodium nitrite;
In
tetrachloromethane; dichloromethane; water; acetonitrile;
DOI:10.1039/c4ob00923a