Technology Process of C15H17NO2
There total 6 articles about C15H17NO2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
triethylamine; trifluoroacetic anhydride;
In
dichloromethane;
at -10 ℃;
DOI:10.1055/s-0030-1260542
- Guidance literature:
-
Multi-step reaction with 2 steps
1: potassium fluoride / isopropyl alcohol / 20 °C
2: triethylamine; trifluoroacetic anhydride / dichloromethane / -10 °C
With
potassium fluoride; triethylamine; trifluoroacetic anhydride;
In
dichloromethane; isopropyl alcohol;
1: Henry reaction;
DOI:10.1055/s-0030-1260542
- Guidance literature:
-
Multi-step reaction with 5 steps
1: bis-triphenylphosphine-palladium(II) chloride / tetrahydrofuran / 20 °C
2: tetrabutyl ammonium fluoride / tetrahydrofuran / 20 °C
4: potassium fluoride / isopropyl alcohol / 20 °C
5: triethylamine; trifluoroacetic anhydride / dichloromethane / -10 °C
With
bis-triphenylphosphine-palladium(II) chloride; potassium fluoride; tetrabutyl ammonium fluoride; triethylamine; trifluoroacetic anhydride;
In
tetrahydrofuran; dichloromethane; isopropyl alcohol;
1: Negishi coupling reaction / 3: Swern oxidation / 4: Henry reaction;
DOI:10.1055/s-0030-1260542