({2-[(1S,2R,4R)-2-Hydroxy-4-methylcyclohexyl]propan-2-yl}amino)acetic acid

Base Information

Chemical Name:({2-[(1S,2R,4R)-2-Hydroxy-4-methylcyclohexyl]propan-2-yl}amino)acetic acid
CAS No.:1277183-24-0
Molecular Formula:C₁₂H₂₃NO₃
Molecular Weight:229.32
Hs Code.:

Synonyms:({2-[(1S,2R,4R)-2-Hydroxy-4-methylcyclohexyl]propan-2-yl}amino)acetic acid

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Chemical Property of ({2-[(1S,2R,4R)-2-Hydroxy-4-methylcyclohexyl]propan-2-yl}amino)acetic acid

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Technology Process of ({2-[(1S,2R,4R)-2-Hydroxy-4-methylcyclohexyl]propan-2-yl}amino)acetic acid

There total 1 articles about ({2-[(1S,2R,4R)-2-Hydroxy-4-methylcyclohexyl]propan-2-yl}amino)acetic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 55179-51-6
(-)-aminomenthol

: 79-08-3
bromoacetic acid

: 1277183-24-0
({2-[(1S,2R,4R)-2-Hydroxy-4-methylcyclohexyl]propan-2-yl}amino)acetic acid

Guidance literature:: With sodium hydroxide; In ethanol; water; at 0 - 90 ℃; pH=12;
DOI:10.1021/jo102213d

Reference yield:

: 1277183-24-0
({2-[(1S,2R,4R)-2-Hydroxy-4-methylcyclohexyl]propan-2-yl}amino)acetic acid

: 1332640-33-1
(1R,6aS,9R,10aR,11aS)-6,6,9-trimethyl-1-(3-phenylprop-1-yn-1-yl)octahydro-6H-[1,4]oxazino[3,4-b][1,3]benzoxazin-3(4H)-one

Guidance literature:: Multi-step reaction with 2 steps

1.1: 1,4-dioxane; water / 1 h / 70 °C

2.1: sodium hydride / tetrahydrofuran; mineral oil / 0.25 h / 0 °C

2.2: -78 - -40 °C

With sodium hydride; In tetrahydrofuran; 1,4-dioxane; water; mineral oil;
DOI:10.1021/jo102213d

Reference yield:

: 1277183-24-0
({2-[(1S,2R,4R)-2-Hydroxy-4-methylcyclohexyl]propan-2-yl}amino)acetic acid

: 1277183-30-8
(1S,6aS,9R,10aR,11aS)-6,6,9-trimethyl-1-(2-phenylethenyl)octahydro-6H-[1,4]oxazino[3,4-b][1,3]benzoxazin-3(4H)-one

Guidance literature:: Multi-step reaction with 3 steps

1.1: 1,4-dioxane; water / 1 h / 70 °C

2.1: sodium hydride / tetrahydrofuran; mineral oil / 0.25 h / 0 °C

2.2: -78 - -40 °C

3.1: N,N,N,N,-tetramethylethylenediamine; hydrogen; nickel(II) acetate tetrahydrate / ethanol / 0 - 20 °C / Inert atmosphere

With N,N,N,N,-tetramethylethylenediamine; hydrogen; nickel(II) acetate tetrahydrate; sodium hydride; In tetrahydrofuran; 1,4-dioxane; ethanol; water; mineral oil;
DOI:10.1021/jo102213d