N-ethoxycarbonyl-1,2,3,4-tetrahydro-6-methoxy-1-(3,4-dimethoxy-benzyl)-isoquinolin-7-ol

Base Information

Chemical Name:N-ethoxycarbonyl-1,2,3,4-tetrahydro-6-methoxy-1-(3,4-dimethoxy-benzyl)-isoquinolin-7-ol
CAS No.:206856-41-9
Molecular Formula:C₂₂H₂₇NO₆
Molecular Weight:401.459
Hs Code.:

Synonyms:N-ethoxycarbonyl-1,2,3,4-tetrahydro-6-methoxy-1-(3,4-dimethoxy-benzyl)-isoquinolin-7-ol

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Chemical Property of N-ethoxycarbonyl-1,2,3,4-tetrahydro-6-methoxy-1-(3,4-dimethoxy-benzyl)-isoquinolin-7-ol

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Technology Process of N-ethoxycarbonyl-1,2,3,4-tetrahydro-6-methoxy-1-(3,4-dimethoxy-benzyl)-isoquinolin-7-ol

There total 2 articles about N-ethoxycarbonyl-1,2,3,4-tetrahydro-6-methoxy-1-(3,4-dimethoxy-benzyl)-isoquinolin-7-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 263360-61-8
N-ethoxycarbonyl-1,2,3,4-tetrahydro-6-methoxy-1-(3,4-dimethoxy-benzyl)-7-phenylmethoxyisoquinoline

: 206856-41-9
N-ethoxycarbonyl-1,2,3,4-tetrahydro-6-methoxy-1-(3,4-dimethoxy-benzyl)-isoquinolin-7-ol

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethyl acetate; at 25 ℃; for 3h; under 760 Torr;
DOI:10.3987/COM-99-S84

Reference yield:

: 59444-68-7
(+/-)-7-benzyloxy-6-methoxy-1-(3,4-dimethoxybenzyl)-1,2,3,4-tetrahydroisoquinoline

: 206856-41-9
N-ethoxycarbonyl-1,2,3,4-tetrahydro-6-methoxy-1-(3,4-dimethoxy-benzyl)-isoquinolin-7-ol

Guidance literature:: Multi-step reaction with 2 steps

1: 81.7 percent / K₂CO₃ / CH₂Cl₂ / 1 h / 25 °C

2: 84 percent / H₂ / 10 percent Pd-C / ethyl acetate / 3 h / 25 °C / 760 Torr

With hydrogen; potassium carbonate; palladium on activated charcoal; In dichloromethane; ethyl acetate; 1: Acylation / 2: debenzylation;
DOI:10.3987/COM-99-S84