5'-deoxy-2',3'-O-isopropylidene-N6-<2-(4-nitrophenyl)ethoxycarbonyl>-5'-<<2-(4-nitrophenyl)ethoxycarbonyl>amino>adenosine

Base Information

Chemical Name:5'-deoxy-2',3'-O-isopropylidene-N6-<2-(4-nitrophenyl)ethoxycarbonyl>-5'-<<2-(4-nitrophenyl)ethoxycarbonyl>amino>adenosine
CAS No.:173097-76-2
Molecular Formula:C₃₁H₃₂N₈O₁₁
Molecular Weight:692.642
Hs Code.:

Synonyms:5'-deoxy-2',3'-O-isopropylidene-N6-<2-(4-nitrophenyl)ethoxycarbonyl>-5'-<<2-(4-nitrophenyl)ethoxycarbonyl>amino>adenosine

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Chemical Property of 5'-deoxy-2',3'-O-isopropylidene-N6-<2-(4-nitrophenyl)ethoxycarbonyl>-5'-<<2-(4-nitrophenyl)ethoxycarbonyl>amino>adenosine

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Technology Process of 5'-deoxy-2',3'-O-isopropylidene-N6-<2-(4-nitrophenyl)ethoxycarbonyl>-5'-<<2-(4-nitrophenyl)ethoxycarbonyl>amino>adenosine

There total 4 articles about 5'-deoxy-2',3'-O-isopropylidene-N6-<2-(4-nitrophenyl)ethoxycarbonyl>-5'-<<2-(4-nitrophenyl)ethoxycarbonyl>amino>adenosine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 88091-70-7
1-methyl-3-[2-(4-nitrophenyl)ethoxycarbonyl]imidazolium chloride

: 21950-36-7
5'-amino-5'-deoxy-2',3'-O-isopropylideneadenosine

: 173097-76-2
5'-deoxy-2',3'-O-isopropylidene-N6-<2-(4-nitrophenyl)ethoxycarbonyl>-5'-<<2-(4-nitrophenyl)ethoxycarbonyl>amino>adenosine

Guidance literature:: In dichloromethane; for 18h; Ambient temperature;
DOI:10.1002/hlca.19950780711

Reference yield:

: 362-75-4
2',3'-isopropylidene adenosine

: 173097-76-2
5'-deoxy-2',3'-O-isopropylidene-N6-<2-(4-nitrophenyl)ethoxycarbonyl>-5'-<<2-(4-nitrophenyl)ethoxycarbonyl>amino>adenosine

Guidance literature:: Multi-step reaction with 4 steps

1: NaHCO₃ / H₂O; pyridine / 18 h / Ambient temperature

2: NaN₃ / dimethylformamide / 0.67 h / 65 - 68 °C

3: conc. NH₄OH, PPh₃ / pyridine / 18 h / Ambient temperature

4: 75 percent / CH₂Cl₂ / 18 h / Ambient temperature

With ammonium hydroxide; sodium azide; sodium hydrogencarbonate; triphenylphosphine; In pyridine; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1002/hlca.19950780711

Reference yield:

: 34245-48-2
5'-azido-5'-deoxy-2',3'-O-isopropylidene adenosine

: 173097-76-2
5'-deoxy-2',3'-O-isopropylidene-N6-<2-(4-nitrophenyl)ethoxycarbonyl>-5'-<<2-(4-nitrophenyl)ethoxycarbonyl>amino>adenosine

Guidance literature:: Multi-step reaction with 2 steps

1: conc. NH₄OH, PPh₃ / pyridine / 18 h / Ambient temperature

2: 75 percent / CH₂Cl₂ / 18 h / Ambient temperature

With ammonium hydroxide; triphenylphosphine; In pyridine; dichloromethane;
DOI:10.1002/hlca.19950780711