*,S^*)>-β-<(2-carboxyethyl)thio>-α-methoxy-2-(8-phenyloctyl)benzenepropanoic acid

Base Information

• Chemical Name: *,S^*)>-β-<(2-carboxyethyl)thio>-α-methoxy-2-(8-phenyloctyl)benzenepropanoic acid
• CAS No.: 121441-85-8
• Molecular Formula: C₂₇H₃₆O₅S
• Molecular Weight: 472.646

Synonyms:*,S^*)>-β-<(2-carboxyethyl)thio>-α-methoxy-2-(8-phenyloctyl)benzenepropanoic acid

Chemical Property of *,S^*)>-β-<(2-carboxyethyl)thio>-α-methoxy-2-(8-phenyloctyl)benzenepropanoic acid

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Technology Process of *,S^*)>-β-<(2-carboxyethyl)thio>-α-methoxy-2-(8-phenyloctyl)benzenepropanoic acid

There total 7 articles about *,S^*)>-β-<(2-carboxyethyl)thio>-α-methoxy-2-(8-phenyloctyl)benzenepropanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

*,S*)>-methyl α-methoxy-β-<(3-methoxy-3-oxopropyl)thio>-2-(8-phenyloctyl)benzenepropanoate (121441-84-7) → *,S*)>-β-<(2-carboxyethyl)thio>-α-methoxy-2-(8-phenyloctyl)benzenepropanoic acid (121441-85-8)

Guidance literature:

With sodium hydroxide; In methanol; for 18h; Ambient temperature;

DOI:10.1021/jo00275a045

Reference yield:

Methyl 2-methoxy-3-hydroxy-3-[2-(8-phenyloctyl)phenyl ]propanoate (121441-81-4,121521-50-4,121521-51-5) → (R*,S*)-β-<(2-carboxyethyl)thio>-α-methoxy-2-(8-phenyloctyl)benzenepropanoic acid (107023-45-0,121441-85-8,121441-88-1,121521-55-9,121521-56-0)

Guidance literature:

Multi-step reaction with 2 steps

1: trifluoroacetic acid / 18 h / Ambient temperature

2: 10percent aq. NaOH / methanol / 18 h

With sodium hydroxide; trifluoroacetic acid; In methanol;

DOI:10.1021/jo00275a045

Reference yield:

Methyl 2-methoxy-3-hydroxy-3-[2-(8-phenyloctyl)phenyl ]propanoate (121441-81-4,121521-50-4,121521-51-5) → (R*,R*)-β-<(2-carboxyethyl)thio>-α-methoxy-2-(8-phenyloctyl)benzenepropanoic acid (107023-45-0,121441-85-8,121441-88-1,121521-55-9,121521-56-0)

Guidance literature:

Multi-step reaction with 2 steps

1: trifluoroacetic acid / 18 h / Ambient temperature

2: 10percent aq. NaOH / methanol / 18 h

With sodium hydroxide; trifluoroacetic acid; In methanol;

DOI:10.1021/jo00275a045

upstream raw materials:

*,S^*)>-methyl α-methoxy-β-<(3-methoxy-3-oxopropyl)thio>-2-(8-phenyloctyl)benzenepropanoate

*,S^*)>-methyl β-hydroxy-α-methoxy-2-(8-phenyloctyl)benzenepropanoate

*,S^*)>-methyl β-(acethylthio)-α-methoxy-2-(8-phenyloctyl)benzenepropanoate

methyl 2-methoxy-3-(2-carbomethoxyethylthio)-3-[2-(8-phenyloctyl)phenyl]propanoate

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