2-10-formylpteroyl)amino>nonanedioic acid dimethyl ester

Base Information

Chemical Name:2-10-formylpteroyl)amino>nonanedioic acid dimethyl ester
CAS No.:113976-36-6
Molecular Formula:C₂₆H₃₂N₈O₆
Molecular Weight:552.59
Hs Code.:

2-<N-(4-amino-4-deoxy-N<sup>10</sup>-formylpteroyl)amino>nonanedioic acid dimethyl ester

Synonyms:2-10-formylpteroyl)amino>nonanedioic acid dimethyl ester

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Chemical Property of 2-10-formylpteroyl)amino>nonanedioic acid dimethyl ester

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Technology Process of 2-10-formylpteroyl)amino>nonanedioic acid dimethyl ester

There total 7 articles about 2-10-formylpteroyl)amino>nonanedioic acid dimethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2104-19-0
azelaic monomethyl ester

: 113976-36-6
2-10-formylpteroyl)amino>nonanedioic acid dimethyl ester

Guidance literature:: Multi-step reaction with 6 steps

1: SOCl₂ / dimethylformamide / 3 h / Heating

2: Br₂, I₂ / SOCl₂; dimethylformamide / 4 h / Irradiation

3: 3.5 h / Ambient temperature

4: NaN₃ / ethanol / 15 h / Heating

5: H₂, aq. HCl / Pd-C / ethanol / 17 h

6: Et₃N / dimethylformamide

With hydrogenchloride; thionyl chloride; sodium azide; hydrogen; bromine; iodine; triethylamine; palladium on activated charcoal; In thionyl chloride; ethanol; N,N-dimethyl-formamide;
DOI:10.1021/jm00402a014

Reference yield:

: 56555-02-3
methyl 9-chloro-9-oxononanoate

: 113976-36-6
2-10-formylpteroyl)amino>nonanedioic acid dimethyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: Br₂, I₂ / SOCl₂; dimethylformamide / 4 h / Irradiation

2: 3.5 h / Ambient temperature

3: NaN₃ / ethanol / 15 h / Heating

4: H₂, aq. HCl / Pd-C / ethanol / 17 h

5: Et₃N / dimethylformamide

With hydrogenchloride; sodium azide; hydrogen; bromine; iodine; triethylamine; palladium on activated charcoal; In thionyl chloride; ethanol; N,N-dimethyl-formamide;
DOI:10.1021/jm00402a014

Reference yield:

: 6415-48-1
2-bromoazelaic acid dimethyl ester

: 113976-36-6
2-10-formylpteroyl)amino>nonanedioic acid dimethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: NaN₃ / ethanol / 15 h / Heating

2: H₂, aq. HCl / Pd-C / ethanol / 17 h

3: Et₃N / dimethylformamide

With hydrogenchloride; sodium azide; hydrogen; triethylamine; palladium on activated charcoal; In ethanol; N,N-dimethyl-formamide;
DOI:10.1021/jm00402a014