ethyl 2-(5-(4-acetamidophenylsulfonamido)-1,3,4-thiadiazol-2-yl)acetate

Base Information

Chemical Name:ethyl 2-(5-(4-acetamidophenylsulfonamido)-1,3,4-thiadiazol-2-yl)acetate
CAS No.:1191951-68-4
Molecular Formula:C₁₄H₁₆N₄O₅S₂
Molecular Weight:384.437
Hs Code.:

Synonyms:ethyl 2-(5-(4-acetamidophenylsulfonamido)-1,3,4-thiadiazol-2-yl)acetate

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Chemical Property of ethyl 2-(5-(4-acetamidophenylsulfonamido)-1,3,4-thiadiazol-2-yl)acetate

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Technology Process of ethyl 2-(5-(4-acetamidophenylsulfonamido)-1,3,4-thiadiazol-2-yl)acetate

There total 2 articles about ethyl 2-(5-(4-acetamidophenylsulfonamido)-1,3,4-thiadiazol-2-yl)acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 88124-55-4
2-Amino-1,3,4-thiadiazolyl-5-acetic acid ethyl ester

: 121-60-8
p-acetylaminobenzenesulfonyl chloride

: 1191951-68-4
ethyl 2-(5-(4-acetamidophenylsulfonamido)-1,3,4-thiadiazol-2-yl)acetate

Guidance literature:: 2-Amino-1,3,4-thiadiazolyl-5-acetic acid ethyl ester; p-acetylaminobenzenesulfonyl chloride; With pyridine; at 20 ℃; for 4.5h;

With hydrogenchloride; In water;
DOI:10.1016/j.bmc.2011.01.049

Reference yield:

: 2318-25-4,165895-16-9
ethyl 3-ethoxy-3-iminopropanoate hydrochloride

: 1191951-68-4
ethyl 2-(5-(4-acetamidophenylsulfonamido)-1,3,4-thiadiazol-2-yl)acetate

Guidance literature:: Multi-step reaction with 2 steps

1: acetic acid / 1.67 h / 55 °C / Reflux

2: pyridine / 4.5 h / 20 °C

With pyridine; acetic acid;
DOI:10.1016/j.bmc.2011.01.049

Reference yield: 88.0%

: 1191951-68-4
ethyl 2-(5-(4-acetamidophenylsulfonamido)-1,3,4-thiadiazol-2-yl)acetate

: 1191951-69-5
2-(5-(4-acetamidophenylsulfonamido)-1,3,4-thiadiazol-2-yl)acetic acid

Guidance literature:: ethyl 2-(5-(4-acetamidophenylsulfonamido)-1,3,4-thiadiazol-2-yl)acetate; With lithium hydroxide; In tetrahydrofuran; water; at 20 ℃; for 24h;

In water; pH=4;
DOI:10.1016/j.bmc.2011.01.049