2-(benzyloxy)-3-methyl-3-(3-(triisopropylsilyl)prop-2-ynyl)isobenzofuran-1(3H)-one O-benzyl oxime

Base Information

• Chemical Name: 2-(benzyloxy)-3-methyl-3-(3-(triisopropylsilyl)prop-2-ynyl)isobenzofuran-1(3H)-one O-benzyl oxime
• CAS No.: 1203447-47-5
• Molecular Formula: C₂₈H₃₇NO₂Si
• Molecular Weight: 447.693
• Mol file: 1203447-47-5.mol

Synonyms:2-(benzyloxy)-3-methyl-3-(3-(triisopropylsilyl)prop-2-ynyl)isobenzofuran-1(3H)-one O-benzyl oxime

Chemical Property of 2-(benzyloxy)-3-methyl-3-(3-(triisopropylsilyl)prop-2-ynyl)isobenzofuran-1(3H)-one O-benzyl oxime

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of 2-(benzyloxy)-3-methyl-3-(3-(triisopropylsilyl)prop-2-ynyl)isobenzofuran-1(3H)-one O-benzyl oxime

There total 1 articles about 2-(benzyloxy)-3-methyl-3-(3-(triisopropylsilyl)prop-2-ynyl)isobenzofuran-1(3H)-one O-benzyl oxime which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 41.0%

N-(benzyloxy)-2-(prop-2-en-2-yl)benzamide (1203447-28-2) + 1-[(triisopropylsilyl)ethynyl]-1,2-benziodoxol-3(1H)-one (181934-30-5) → 2-(benzyloxy)-3-methyl-3-(3-(triisopropylsilyl)prop-2-ynyl)isobenzofuran-1(3H)-one O-benzyl oxime (1203447-47-5) + 2-(benzyloxy)-3-methyl-3-(3-(triisopropylsilyl)prop-2-ynyl)isoindolin-1-one (1203447-46-4)

Guidance literature:

With palladium(II) hexafluoroacetylacetonate; In dichloromethane; at 23 ℃; for 12h; Inert atmosphere;

DOI:10.1021/ol9027286

upstream raw materials:

N-(benzyloxy)-2-(prop-2-en-2-yl)benzamide

1-[(triisopropylsilyl)ethynyl]-1,2-benziodoxol-3(1H)-one