(2R,3R,4S)-4-(4-methoxybenzyloxy)-tetrahydro-2-(3,4-dihydro-2,4-dioxopyrimidin-1(2H)-yl)furan-3-yl acetate

Base Information

Chemical Name:(2R,3R,4S)-4-(4-methoxybenzyloxy)-tetrahydro-2-(3,4-dihydro-2,4-dioxopyrimidin-1(2H)-yl)furan-3-yl acetate
CAS No.:1333503-53-9
Molecular Formula:C₁₈H₂₀N₂O₇
Molecular Weight:376.366
Hs Code.:

Synonyms:(2R,3R,4S)-4-(4-methoxybenzyloxy)-tetrahydro-2-(3,4-dihydro-2,4-dioxopyrimidin-1(2H)-yl)furan-3-yl acetate

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Chemical Property of (2R,3R,4S)-4-(4-methoxybenzyloxy)-tetrahydro-2-(3,4-dihydro-2,4-dioxopyrimidin-1(2H)-yl)furan-3-yl acetate

Chemical Property:

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Technology Process of (2R,3R,4S)-4-(4-methoxybenzyloxy)-tetrahydro-2-(3,4-dihydro-2,4-dioxopyrimidin-1(2H)-yl)furan-3-yl acetate

There total 1 articles about (2R,3R,4S)-4-(4-methoxybenzyloxy)-tetrahydro-2-(3,4-dihydro-2,4-dioxopyrimidin-1(2H)-yl)furan-3-yl acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1333503-49-3
(3R,4S)-4-(4-methoxybenzyloxy)-tetrahydrofuran-2,3-diyl diacetate

: 10457-14-4
O,O'-bis-(trimethylsilyl)uracil

: 1333503-53-9
(2R,3R,4S)-4-(4-methoxybenzyloxy)-tetrahydro-2-(3,4-dihydro-2,4-dioxopyrimidin-1(2H)-yl)furan-3-yl acetate

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; In 1,2-dichloro-ethane; at 0 - 20 ℃; for 4h; Inert atmosphere;
DOI:10.1016/j.ejmech.2011.05.036

Reference yield: 90.0%

: 1333503-53-9
(2R,3R,4S)-4-(4-methoxybenzyloxy)-tetrahydro-2-(3,4-dihydro-2,4-dioxopyrimidin-1(2H)-yl)furan-3-yl acetate

: 1333503-59-5
1-((2R,3R,4S)-4-(4-methoxybenzyloxy)-tetrahydro-3-hydroxyfuran-2-yl)pyrimidine-2,4(1H,3H)-dione

Guidance literature:: With methanol; ammonia; at 20 ℃; for 6h; Inert atmosphere;
DOI:10.1016/j.ejmech.2011.05.036

Reference yield:

: 1333503-53-9
(2R,3R,4S)-4-(4-methoxybenzyloxy)-tetrahydro-2-(3,4-dihydro-2,4-dioxopyrimidin-1(2H)-yl)furan-3-yl acetate

: C₂₄H₂₄N₂O₇S

Guidance literature:: Multi-step reaction with 2 steps

1: methanol; ammonia / 6 h / 20 °C / Inert atmosphere

2: dmap / acetonitrile / 0 - 20 °C / Inert atmosphere

With methanol; dmap; ammonia; In acetonitrile;
DOI:10.1016/j.ejmech.2011.05.036