methyl (2,3,6-tri-O-benzoyl-4-deoxy-β-D-xylo-hexopyranosyl)-(1->4)-[2,3,4-tri-O-benzyl-α-L-fucopyranosyl-(1->3)]-6-O-benzyl-2-deoxy-2-phthalimido-β-D-glucopyranos

Base Information

Chemical Name:methyl (2,3,6-tri-O-benzoyl-4-deoxy-β-D-xylo-hexopyranosyl)-(1->4)-[2,3,4-tri-O-benzyl-α-L-fucopyranosyl-(1->3)]-6-O-benzyl-2-deoxy-2-phthalimido-β-D-glucopyranos
CAS No.:1257791-12-0
Molecular Formula:C₇₆H₇₃NO₁₈
Molecular Weight:1288.41
Hs Code.:

methyl (2,3,6-tri-O-benzoyl-4-deoxy-β-D-xylo-hexopyranosyl)-(1->4)-[2,3,4-tri-O-benzyl-α-L-fucopyranosyl-(1->3)]-6-O-benzyl-2-deoxy-2-phthalimido-β-D-glucopyranos

Synonyms:methyl (2,3,6-tri-O-benzoyl-4-deoxy-β-D-xylo-hexopyranosyl)-(1->4)-[2,3,4-tri-O-benzyl-α-L-fucopyranosyl-(1->3)]-6-O-benzyl-2-deoxy-2-phthalimido-β-D-glucopyranos

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Chemical Property of methyl (2,3,6-tri-O-benzoyl-4-deoxy-β-D-xylo-hexopyranosyl)-(1->4)-[2,3,4-tri-O-benzyl-α-L-fucopyranosyl-(1->3)]-6-O-benzyl-2-deoxy-2-phthalimido-β-D-glucopyranos

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Technology Process of methyl (2,3,6-tri-O-benzoyl-4-deoxy-β-D-xylo-hexopyranosyl)-(1->4)-[2,3,4-tri-O-benzyl-α-L-fucopyranosyl-(1->3)]-6-O-benzyl-2-deoxy-2-phthalimido-β-D-glucopyranos

There total 1 articles about methyl (2,3,6-tri-O-benzoyl-4-deoxy-β-D-xylo-hexopyranosyl)-(1->4)-[2,3,4-tri-O-benzyl-α-L-fucopyranosyl-(1->3)]-6-O-benzyl-2-deoxy-2-phthalimido-β-D-glucopyranos which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

: 1257791-11-9
methyl (2,3,6-tri-O-benzoyl-4-deoxy-β-D-xylo-hexopyranosyl)-(1->4)-3-O-acetyl-6-O-benzyl-2-deoxy-2-phthalimido-β-D-glucopyranoside

: 116514-50-2,128962-63-0,131545-02-3,136758-06-0,99409-34-4,116391-11-8
ethyl 2,3,4-tri-O-benzyl-1-thio-β-L-fucopyranoside

: 1257791-12-0
methyl (2,3,6-tri-O-benzoyl-4-deoxy-β-D-xylo-hexopyranosyl)-(1->4)-[2,3,4-tri-O-benzyl-α-L-fucopyranosyl-(1->3)]-6-O-benzyl-2-deoxy-2-phthalimido-β-D-glucopyranos

Guidance literature:: With N-iodo-succinimide; trifluorormethanesulfonic acid; In toluene; at -30 ℃; for 0.333333h; stereoselective reaction; Inert atmosphere; Molecular sieve;
DOI:10.1007/s11426-010-4060-6

Reference yield:

: 1257791-12-0
methyl (2,3,6-tri-O-benzoyl-4-deoxy-β-D-xylo-hexopyranosyl)-(1->4)-[2,3,4-tri-O-benzyl-α-L-fucopyranosyl-(1->3)]-6-O-benzyl-2-deoxy-2-phthalimido-β-D-glucopyranos

: 108-24-7
acetic anhydride

: C₅₅H₆₇NO₁₇

Guidance literature:: methyl (2,3,6-tri-O-benzoyl-4-deoxy-β-D-xylo-hexopyranosyl)-(1->4)-[2,3,4-tri-O-benzyl-α-L-fucopyranosyl-(1->3)]-6-O-benzyl-2-deoxy-2-phthalimido-β-D-glucopyranos; With water; hydrazine hydrate; In ethanol; for 15h; Reflux;

acetic anhydride; With pyridine; at 30 ℃; for 12h;
DOI:10.1007/s11426-010-4060-6