4-(N,N-Dimethylamino)benzenediazonium chloride

Base Information

• Chemical Name: 4-(N,N-Dimethylamino)benzenediazonium chloride
• CAS No.: 100-04-9
• Deprecated CAS: 1323352-69-7
• Molecular Formula: C8H10ClN3
• Molecular Weight: 183.64
• Hs Code.: 2927000090
• European Community (EC) Number: 202-813-8
• DSSTox Substance ID: DTXSID60883290
• Mol file: 100-04-9.mol

Synonyms:4-dimethylaminobenzenediazonium chloride;4-dimethylaminobenzenediazonium fluoroborate;4-dimethylaminobenzenediazonium hexafluorophosphate (1-);4-dimethylaminobenzenediazonium perchlorate;4-dimethylaminobenzenediazonium sulfite (1:1), sodium salt;4-dimethylaminobenzenediazonium trichlorozincate (1-);4-dimethylaminobenzenediazonium, (T-4)-tetrachlorozincate (2-) (2:1);4-N,N-dimethylaminobenzene diazonium chloride;DDFB;p-(n,N-dimethyl)aminobenzenediazonium fluoroborate;para-dimethylaminobenzene diazonium fluoroborate

Chemical Property of 4-(N,N-Dimethylamino)benzenediazonium chloride

Chemical Property:

• PSA: 31.39000
• LogP: -0.75882
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 1
• Exact Mass: 183.0563250
• Heavy Atom Count: 12
• Complexity: 159

Purity/Quality:

98%,99%, ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CN(C)C1=CC=C(C=C1)[N+]#N.[Cl-]

Technology Process of 4-(N,N-Dimethylamino)benzenediazonium chloride

There total 6 articles about 4-(N,N-Dimethylamino)benzenediazonium chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-dimethylaminophenylamine dihydrochloride (536-46-9,13806-04-7) + isopentyl nitrite (110-46-3) → p-dimethylaminobenzenediazonium chloride (100-04-9)

Guidance literature:

With ethanol;

Reference yield:

N,N-dimethyl-1,4-phenylenediamine sulfate (536-47-0) → p-dimethylaminobenzenediazonium chloride (100-04-9)

Guidance literature:

With hydrogenchloride; sodium nitrite; In water;

DOI:10.1007/BF00506048

Reference yield:

4-amino-N,N-dimethylaniline (99-98-9) → p-dimethylaminobenzenediazonium chloride (100-04-9)

Guidance literature:

With sodium nitrite; In hydrogenchloride;

DOI:10.1002/omr.1270210710

upstream raw materials:

4-dimethylaminophenylamine dihydrochloride

isopentyl nitrite

N,N-dimethyl-1,4-phenylenediamine sulfate

4-amino-N,N-dimethylaniline

Downstream raw materials:

4-(azulen-1-yl-trans-azo)-N,N-dimethyl-aniline

(4-N,N-dimethyl-aminophenyl)-(4N-methyl-pyridinio)-acetylene iodide

p-(dimethylamino)phenyl azide

Refernces

• 1、 Jonassen et al.. "". . p. 595,596. Retrieved 1964.
• 2、 -. "Surface Functionalisation Using Arylcarbene Reactive Intermediates". . . Retrieved 2008/12/06.
• 3、 Dunn, III, W.J.,Lins, C.,Kumar, G.,Manimaran, T.,Grigoras, S.,et al.. "Substituent Effects on 13C and 15N Chemical Shifts in Triazenes Studied by Principal Components Multivariate Data Analysis". . p. 450 - 456. Retrieved 2007/10/02.