2-anilinoethyl-3-chloropropionate-{2-[ethyl[4-[(4'-nitrophenyl)azo]phenyl]amino]ethanol}

Base Information

Chemical Name:2-anilinoethyl-3-chloropropionate-{2-[ethyl[4-[(4'-nitrophenyl)azo]phenyl]amino]ethanol}
CAS No.:1447102-88-6
Molecular Formula:C₂₇H₃₁N₅O₅
Molecular Weight:505.574
Hs Code.:

Synonyms:2-anilinoethyl-3-chloropropionate-{2-[ethyl[4-[(4'-nitrophenyl)azo]phenyl]amino]ethanol}

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Chemical Property of 2-anilinoethyl-3-chloropropionate-{2-[ethyl[4-[(4'-nitrophenyl)azo]phenyl]amino]ethanol}

Chemical Property:

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Technology Process of 2-anilinoethyl-3-chloropropionate-{2-[ethyl[4-[(4'-nitrophenyl)azo]phenyl]amino]ethanol}

There total 2 articles about 2-anilinoethyl-3-chloropropionate-{2-[ethyl[4-[(4'-nitrophenyl)azo]phenyl]amino]ethanol} which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 1447102-83-1
2-anilinoethyl-3-chloropropionate

: 2872-52-8
disperse red 1

: 1447102-88-6
2-anilinoethyl-3-chloropropionate-{2-[ethyl[4-[(4'-nitrophenyl)azo]phenyl]amino]ethanol}

Guidance literature:: disperse red 1; With potassium; In tetrahydrofuran; at 75 ℃; for 5h; Inert atmosphere; Reflux;

2-anilinoethyl-3-chloropropionate; In tetrahydrofuran; at 20 ℃; for 28h; Inert atmosphere; Reflux;
DOI:10.1080/15533174.2012.750345

Reference yield:

: 92-50-2
2-( N-ethylanilino)ethanol

: 100-01-6,104810-17-5
4-nitro-aniline

: 1447102-88-6
2-anilinoethyl-3-chloropropionate-{2-[ethyl[4-[(4'-nitrophenyl)azo]phenyl]amino]ethanol}

Guidance literature:: Multi-step reaction with 2 steps

1.1: hydrogenchloride / water / 0.25 h / 30 °C

1.2: 0.5 h

1.3: 0.5 h / 0 °C

2.1: potassium / tetrahydrofuran / 5 h / 75 °C / Inert atmosphere; Reflux

2.2: 28 h / 20 °C / Inert atmosphere; Reflux

With hydrogenchloride; potassium; In tetrahydrofuran; water;
DOI:10.1080/15533174.2012.750345