2,4,6-trimethylphenylgermanium trihydride

Base Information

Chemical Name:2,4,6-trimethylphenylgermanium trihydride
CAS No.:72876-20-1
Molecular Formula:C₉H₁₄Ge
Molecular Weight:194.8
Hs Code.:

Synonyms:2,4,6-trimethylphenylgermanium trihydride

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Chemical Property of 2,4,6-trimethylphenylgermanium trihydride

Chemical Property:

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Technology Process of 2,4,6-trimethylphenylgermanium trihydride

There total 11 articles about 2,4,6-trimethylphenylgermanium trihydride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 143880-59-5
mesityldihydrogermyllithium

: mercury dichloride

: 72876-20-1
2,4,6-trimethylphenylgermanium trihydride

: {((CH₃)3C₆H₂)HGe}(x)

: 143880-66-4
1,2-dimesityl 1,2-digermane

: mercury

Guidance literature:: In tetrahydrofuran; byproducts: LiCl; under inert atm.; HgCl2 added in portions at-60°C within 1 h; at ambient temp. for 12 h; heated at 40°C for 3 h; Hg isolated by decantation; soln. hydrolyzed; extd. (ether); dried; concd. (reduced pressure); NMR;
DOI:10.1016/0022-328X(92)80129-L

Reference yield: 86.0%

: 10038-98-9
germaniumtetrachloride

: 2633-66-1
2-mesitylmagnesium bromide

: 72876-20-1
2,4,6-trimethylphenylgermanium trihydride

: 72876-19-8
bis(2,4,6-trimethylphenyl)germane

Guidance literature:: With lithium aluminium tetrahydride; In diethyl ether; dry/inert atmosphere; stirring (6 h), slow addn. of LiAlH4 (cooling); aq. HCl addn., ether layer evapn., distn.;
DOI:10.1080/00945719608004362