p-tolyl 4,6-O-benzylidene-2-deoxy-2-trichloroacetamido-1-thio-β-D-glucopyranoside

Base Information

Chemical Name:p-tolyl 4,6-O-benzylidene-2-deoxy-2-trichloroacetamido-1-thio-β-D-glucopyranoside
CAS No.:929040-54-0
Molecular Formula:C₂₂H₂₂Cl₃NO₅S
Molecular Weight:518.845
Hs Code.:

Synonyms:p-tolyl 4,6-O-benzylidene-2-deoxy-2-trichloroacetamido-1-thio-β-D-glucopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of p-tolyl 4,6-O-benzylidene-2-deoxy-2-trichloroacetamido-1-thio-β-D-glucopyranoside

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Technology Process of p-tolyl 4,6-O-benzylidene-2-deoxy-2-trichloroacetamido-1-thio-β-D-glucopyranoside

There total 1 articles about p-tolyl 4,6-O-benzylidene-2-deoxy-2-trichloroacetamido-1-thio-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₅H₁₈Cl₃NO₅S

: 1125-88-8
benzaldehyde dimethyl acetal

: 929040-54-0
p-tolyl 4,6-O-benzylidene-2-deoxy-2-trichloroacetamido-1-thio-β-D-glucopyranoside

Guidance literature:: With camphor-10-sulfonic acid; In toluene; at 80 ℃; for 1h; Inert atmosphere;
DOI:10.1021/jo9016925

Reference yield: 80.0%

: 929040-56-2
p-tolyl 2-O-benzoyl-3-O-benzyl-4-O-tert-butyldimethylsilyl-6-O-p-methoxybenzyl-1-thio-β-D-glucopyranoside

: 929040-54-0
p-tolyl 4,6-O-benzylidene-2-deoxy-2-trichloroacetamido-1-thio-β-D-glucopyranoside

: 1191081-71-6
p-tolyl O-(2-O-benzoyl-3-O-benzyl-4-O-tert-butyldimethylsilyl-6-O-p-methoxybenzyl-β-D-glucopyranosyl)-(1->3)-4,6-O-benzylidene-2-deoxy-1-thio-2-trichloroacetamido-β-D-glucopyranoside

Guidance literature:: p-tolyl 2-O-benzoyl-3-O-benzyl-4-O-tert-butyldimethylsilyl-6-O-p-methoxybenzyl-1-thio-β-D-glucopyranoside; With p-methylbenzenesulfenyl chloride; silver trifluoromethanesulfonate; In diethyl ether; at -78 ℃; for 0.0833333h; Molecular sieve;

p-tolyl 4,6-O-benzylidene-2-deoxy-2-trichloroacetamido-1-thio-β-D-glucopyranoside; With 2,4,6-tri-tert-butylpyrimidine; In diethyl ether; dichloromethane; acetonitrile; at -78 - -10 ℃;
DOI:10.1021/jo9016925

Reference yield: 80.0%

: 929040-54-0
p-tolyl 4,6-O-benzylidene-2-deoxy-2-trichloroacetamido-1-thio-β-D-glucopyranoside

: 4-methylphenyl 2-O-benzoyl-4,6-di-O-benzyl-3-O-(naphthalene-2-ylmethyl)-1-thio-β-D-galactopyranoside

: 4-methylphenyl(2-O-benzoyl-4,6-di-O-benzyl-3-O-(naphthalen-2-ylmethyl)-β-D-galactopyranosyl)-(1→3)-4,6-O-benzylidene-2-deoxy-2-trichloroacetamido-1-thio-β-D-glucopyranoside

Guidance literature:: With N-iodo-succinimide; trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at -60 ℃; for 4h; chemoselective reaction; Inert atmosphere; Molecular sieve;
DOI:10.1021/acs.joc.0c02422