C₂₆H₃₂N₂O

Base Information

Chemical Name:C₂₆H₃₂N₂O
CAS No.:378244-01-0
Molecular Formula:C₂₆H₃₂N₂O
Molecular Weight:388.553
Hs Code.:

C<sub>26</sub>H<sub>32</sub>N<sub>2</sub>O

Synonyms:C₂₆H₃₂N₂O

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Chemical Property of C₂₆H₃₂N₂O

Chemical Property:

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Technology Process of C₂₆H₃₂N₂O

There total 18 articles about C₂₆H₃₂N₂O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 378244-00-9
4-benzyloxymethyl-6-ethyl-2-[3-(2-oxo-ethyl)-1H-indol-2-yl]-azepane-1-carboxylic acid tert-butyl ester

: 378244-01-0
C₂₆H₃₂N₂O

Guidance literature:: 4-benzyloxymethyl-6-ethyl-2-[3-(2-oxo-ethyl)-1H-indol-2-yl]-azepane-1-carboxylic acid tert-butyl ester; With boron trifluoride; acetic acid; at 0 ℃;

With sodium cyanoborohydride;
DOI:10.1016/S0040-4039(01)01538-6

Reference yield:

: 193558-26-8
3-oxotricyclo[4.2.1.0^2.5]non-7-ene

: 378244-01-0
C₂₆H₃₂N₂O

Guidance literature:: Multi-step reaction with 18 steps

1.1: 93 percent / OsO₄; 4-methylmorpholine N-oxide

2.1: 57 percent / Irradiation

3.1: 99 percent / H₂ / PtO₂ / ethyl acetate

4.1: NaIO₄

4.2: NaBH₄

5.1: Et₃N

6.1: NaN₃ / dimethylformamide / 80 °C

7.1: 95 percent / H₂; NH₃ / Pd-C / methanol

8.1: 84 percent / NaH / tetrahydrofuran

9.1: 100 percent / t-BuLi / -78 °C

10.1: LiEt₃BH / -78 °C

10.2: 78 percent / HCl

11.1: BuLi; Me₂AlCl / CH₂Cl₂ / -78 - 0 °C

11.2: 75 percent / TBAF

12.1: 89 percent / CuI; Et₃N / (Ph₃P)2PdCl₂ / Heating

13.1: 65 percent / NaOEt / ethanol / Heating

14.1: dimethylformamide / 100 °C

15.1: DIBAL / -78 °C

15.2: 92 percent / H₂SO₄ / H₂O

16.1: BF₃; AcOH / 0 °C

16.2: 60 percent / NaBH₃CN

With sodium periodate; copper(l) iodide; osmium(VIII) oxide; n-butyllithium; sodium azide; boron trifluoride; ammonia; hydrogen; tert.-butyl lithium; sodium ethanolate; dimethylaluminum chloride; sodium hydride; diisobutylaluminium hydride; lithium triethylborohydride; acetic acid; 4-methylmorpholine N-oxide; triethylamine; platinum(IV) oxide; bis-triphenylphosphine-palladium(II) chloride; palladium on activated charcoal; In tetrahydrofuran; methanol; ethanol; dichloromethane; ethyl acetate; N,N-dimethyl-formamide; 12.1: Sonogashira reaction;
DOI:10.1016/S0040-4039(01)01538-6

Reference yield:

: 378243-88-0
(R)-4-((R)-2-Hydroxymethyl-butyl)-dihydro-furan-2-one

: 378244-01-0
C₂₆H₃₂N₂O

Guidance literature:: Multi-step reaction with 14 steps

1.1: Et₃N

2.1: NaN₃ / dimethylformamide / 80 °C

3.1: 95 percent / H₂; NH₃ / Pd-C / methanol

4.1: 84 percent / NaH / tetrahydrofuran

5.1: 100 percent / t-BuLi / -78 °C

6.1: LiEt₃BH / -78 °C

6.2: 78 percent / HCl

7.1: BuLi; Me₂AlCl / CH₂Cl₂ / -78 - 0 °C

7.2: 75 percent / TBAF

8.1: 89 percent / CuI; Et₃N / (Ph₃P)2PdCl₂ / Heating

9.1: 65 percent / NaOEt / ethanol / Heating

10.1: dimethylformamide / 100 °C

11.1: DIBAL / -78 °C

11.2: 92 percent / H₂SO₄ / H₂O

12.1: BF₃; AcOH / 0 °C

12.2: 60 percent / NaBH₃CN

With copper(l) iodide; n-butyllithium; sodium azide; boron trifluoride; ammonia; hydrogen; tert.-butyl lithium; sodium ethanolate; dimethylaluminum chloride; sodium hydride; diisobutylaluminium hydride; lithium triethylborohydride; acetic acid; triethylamine; bis-triphenylphosphine-palladium(II) chloride; palladium on activated charcoal; In tetrahydrofuran; methanol; ethanol; dichloromethane; N,N-dimethyl-formamide; 8.1: Sonogashira reaction;
DOI:10.1016/S0040-4039(01)01538-6