3-(3-nitrobenzoylformamido)-4-(3-nitrophenyl)-1,2,5-thiadiazole

Base Information

• Chemical Name: 3-(3-nitrobenzoylformamido)-4-(3-nitrophenyl)-1,2,5-thiadiazole
• CAS No.: 163430-78-2
• Molecular Formula: C₁₆H₉N₅O₆S
• Molecular Weight: 399.343
• Mol file: 163430-78-2.mol

Synonyms:3-(3-nitrobenzoylformamido)-4-(3-nitrophenyl)-1,2,5-thiadiazole

Chemical Property of 3-(3-nitrobenzoylformamido)-4-(3-nitrophenyl)-1,2,5-thiadiazole

Chemical Property:

Purity/Quality:

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Technology Process of 3-(3-nitrobenzoylformamido)-4-(3-nitrophenyl)-1,2,5-thiadiazole

There total 1 articles about 3-(3-nitrobenzoylformamido)-4-(3-nitrophenyl)-1,2,5-thiadiazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2,2-dibromo-1-(3-nitrophenyl)ethan-1-one (13651-07-5) → 2,5-bis(3-nitrobenzoyl)-1,2,4-thiadiazole + 3-(3-nitrobenzoylformamido)-4-(3-nitrophenyl)-1,2,5-thiadiazole (163430-78-2)

Guidance literature:

With tetrasulphur tetranitride; at 115 ℃; for 10h;

Reference yield: 89.0%

3-(3-nitrobenzoylformamido)-4-(3-nitrophenyl)-1,2,5-thiadiazole (163430-78-2) → 3-amino-4-(3-nitrophenyl)-1,2,5-thiadiazole

Guidance literature:

With sodium tetrahydroborate; In ethanol; chloroform; for 1h; Ambient temperature;

Reference yield: 59.0%

3-(3-nitrobenzoylformamido)-4-(3-nitrophenyl)-1,2,5-thiadiazole (163430-78-2) → 2,5-bis(3-nitrobenzoyl)-1,2,4-thiadiazole

Guidance literature:

With 3-chloro-benzenecarboperoxoic acid; In chloroform; for 7h; Ambient temperature;

upstream raw materials:

2,2-dibromo-1-(3-nitrophenyl)ethan-1-one