(2S,3R,4Z)-6-tert-butyldimethylsilyloxy-3-ethyl-2-hydroxy-4-hexenyl benzoate

Base Information

Chemical Name:(2S,3R,4Z)-6-tert-butyldimethylsilyloxy-3-ethyl-2-hydroxy-4-hexenyl benzoate
CAS No.:216174-61-7
Molecular Formula:C₂₁H₃₄O₄Si
Molecular Weight:378.584
Hs Code.:

Synonyms:(2S,3R,4Z)-6-tert-butyldimethylsilyloxy-3-ethyl-2-hydroxy-4-hexenyl benzoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2S,3R,4Z)-6-tert-butyldimethylsilyloxy-3-ethyl-2-hydroxy-4-hexenyl benzoate

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Technology Process of (2S,3R,4Z)-6-tert-butyldimethylsilyloxy-3-ethyl-2-hydroxy-4-hexenyl benzoate

There total 5 articles about (2S,3R,4Z)-6-tert-butyldimethylsilyloxy-3-ethyl-2-hydroxy-4-hexenyl benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 216174-78-6
(2S,3R)-6-tert-butyldimethylsilyloxy-3-ethyl-2-hydroxy-4-hexynyl benzoate

: 216174-61-7
(2S,3R,4Z)-6-tert-butyldimethylsilyloxy-3-ethyl-2-hydroxy-4-hexenyl benzoate

Guidance literature:: With hydrogen; Lindlar catalyst; In methanol; Ambient temperature;
DOI:10.1016/S0040-4039(98)01860-7

Reference yield:

: 94424-88-1
(2R,3R)-3-(ethyloxiran-2-yl)methanol

: 216174-61-7
(2S,3R,4Z)-6-tert-butyldimethylsilyloxy-3-ethyl-2-hydroxy-4-hexenyl benzoate

Guidance literature:: Multi-step reaction with 3 steps

1: 100 percent / 4-dimethylaminopyridine, Et₃N / CH₂Cl₂ / 0.5 h / 0 °C

3: 100 percent / H₂ / Lindlar catalyst / methanol / 3 h / Ambient temperature

With dmap; hydrogen; triethylamine; Lindlar's catalyst; In methanol; dichloromethane;
DOI:10.1016/S0040-4020(99)00556-6

Reference yield:

: 216174-60-6
(2R,3R)-2,3-epoxypentyl benzoate

: 216174-61-7
(2S,3R,4Z)-6-tert-butyldimethylsilyloxy-3-ethyl-2-hydroxy-4-hexenyl benzoate

Guidance literature:: Multi-step reaction with 2 steps

2: 100 percent / H₂ / Lindlar catalyst / methanol / 3 h / Ambient temperature

With hydrogen; Lindlar's catalyst; In methanol;
DOI:10.1016/S0040-4020(99)00556-6